Adhesive, its preparation method and application method
A technology of adhesives and toughening agents, applied in the direction of adhesives, chemical instruments and methods, adhesive types, etc., can solve the problem of low initial viscosity of adhesives, achieve wide use temperature range, high bonding strength, The effect of improving appearance performance
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[0028] The present invention also discloses a preparation method of the above-mentioned adhesive, including: mixing the main resin, toughening agent and filler, grinding and defoaming to obtain a resin component; and using a normal temperature curing agent as the curing component to obtain the adhesive. The above-mentioned mixing and grinding methods are well-known in the art, for example, they can be rolled into a uniform paste on a three-roll mill.
[0029] In the above method, when one or more of the coupling agent, thixotropic agent, and heat-resistant agent is contained, one or more of the coupling agent, thixotropic agent, and heat-resistant agent can be combined with the host resin , Toughener and filler are mixed together, ground and defoamed to obtain resin component. Similarly, when it is necessary to use a high temperature curing agent and a curing accelerator, it also includes mixing the high temperature curing agent and the curing accelerator with the normal temperat...
Example Embodiment
[0034] Example 1
[0035] This example is used to illustrate the adhesive disclosed in the present invention and its preparation method.
[0036] Combine 80 parts by weight of epoxy resin E-42 (produced by Guangzhou Hongchang Company, with an epoxy equivalent of 280) and 20 parts by weight of epoxy resin E-12 (produced by Guangzhou Hongchang Company, with an epoxy equivalent of 655 and a softening point of 80 °C) mixed with 12 parts by weight of barite, 20 parts by weight of epoxy soybean oil, and 2 parts by weight of aminopropyltriethoxysilane, rolled into a uniform paste on a three-roll mill and defoamed to obtain a resin component .
[0037] Take 15 parts by weight of triethylenetetramine as the curing component. The above-mentioned resin component and curing component together constitute the adhesive S1.
Example Embodiment
[0038] Example 2
[0039] This example is used to illustrate the adhesive disclosed in the present invention and its preparation method.
[0040] The epoxy resin with epoxy equivalent of 180, epoxy resin with epoxy equivalent of 475, and amino-terminated polyetheramine are mixed uniformly in a weight ratio of 80:20:50, and then rapidly stirred at 150°C for 2h to obtain amino-terminated Polyetheramine modified epoxy resin prepolymer.
[0041] Combine 60 parts by weight of epoxy resin E-54 (produced by Guangzhou Hongchang Company, with an epoxy equivalent of 180) and 40 parts by weight of epoxy resin E-12 (produced by Guangzhou Hongchang Company, with an epoxy equivalent of 655 and a softening point of 80 ℃) with 15 parts by weight of calcium carbonate, 18 parts by weight of amino-terminated polyetheramine modified epoxy resin prepolymer, 8 parts by weight of polyurethane (isocyanate equivalent of 2000), 10 parts by weight of carboxyl-terminated nitrile rubber (acrylonitrile content ...
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