Multifunctional comfort fiber with functions of phase transition temperature regulation, moisture absorption and moisture wicking
A moisture-wicking, multi-functional technology, applied in the field of comfort fibers, to avoid the loss of phase change enthalpy, obvious moisture-wicking, low leakage effect
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Embodiment 1
[0029] ① Preparation of interpenetrating network composite phase change materials: N-methylolacrylamide is used as network monomer, N, N-methylenebisacrylamide is used as crosslinking agent, ammonium persulfate is used as initiator, polyethylene glycol is a phase change material.
[0030] Wherein, cross-linking agent 1.5g, monomer 8g, initiator 0.3g, polyethylene glycol (molecular weight 2000) 24g, water 50ml.
[0031] The network monomer, cross-linking agent, polyethylene glycol and solvent water are weighed and reset in the flask according to the above ratio. After dissolving, ultrasonically disperse for 5 minutes, add the initiator, disperse at 30°C for 5 minutes, and then transfer to 75°C React in a water bath for 3 hours, and then dry at a low temperature of 30°C.
[0032] ② Phase-change temperature-regulating fiber preparation: Polyethylene glycol acrylate is used as a compatibilizer, and the composite phase-change material and polypropylene are melt-blended and spun in...
Embodiment 2
[0037] ① Preparation of interpenetrating network composite phase change material: as in Example 1.
[0038] ② Phase-change temperature-regulating fiber preparation: Polyethylene glycol acrylate is used as a compatibilizer, and the composite phase-change material and polypropylene are melt-blended and spun in a screw extruder in proportion to obtain a phase-change temperature-regulating fiber. Geometric parameters of screw extruder: D, 20mm; L / D, 25; process parameters: speed, 35r / min; ℃.
[0039] Among them, 7.5g of composite phase change material, 42.5g of polypropylene, and 2.5g of polyethylene glycol acrylate.
Embodiment 3
[0041] ① Preparation of interpenetrating network composite phase change material: as in Example 1.
[0042] ② Phase-change temperature-regulating fiber preparation: Polyethylene glycol acrylate is used as a compatibilizer, and the composite phase-change material and polypropylene are melt-blended and spun in a screw extruder in proportion to obtain a phase-change temperature-regulating fiber. Geometric parameters of screw extruder: D, 20mm; L / D, 25; process parameters: speed, 35r / min; ℃.
[0043] Among them, 5g of composite phase change material, 45g of polypropylene, and 2.5g of polyethylene glycol acrylate.
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