Looking for breakthrough ideas for innovation challenges? Try Patsnap Eureka!

Synthetic process of alkene monomer

A technology for the synthesis of vinyl monomers and synthesis techniques, which is applied in the field of synthesis techniques of vinyl monomers. It can solve the problems of high cost, large dosage, and large chelation stability constant, and achieve high synthesis yields, reduced production costs, and anti-fouling. good performance effect

Inactive Publication Date: 2012-05-16
袁俊海
View PDF0 Cites 0 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Amino polycarboxylates have large chelation stability constants and can be used at higher temperatures, but they are used in large quantities and cost high; organic polyphosphonic acids have no anti-scaling effect on barium sulfate and strontium sulfate; most of them use organic polymers for anti-scaling. Scale agent, mostly use monomers to copolymerize with maleic anhydride and acrylic acid in order to improve the anti-fouling rate, but because the polymer structure is not fundamentally changed, the expected anti-fouling effect cannot be achieved

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0026] The synthetic technique of the ethylenic monomer that the present invention relates to comprises the following steps:

[0027] (a) raw material is dissolved in solvent, and fully dissolve;

[0028] (b) add catalyst, stir to allow it to fully mix;

[0029] (c) After reacting for a period of time, a reaction product mixture is obtained;

[0030] (d) cooling the reaction product mixture to room temperature, after carrying out vacuum distillation, washing the liquid after distillation;

[0031] (e) separating and drying the washed and distilled liquid to obtain vinyl monomers.

[0032] In said step (d), after the reaction product mixture is cooled to room temperature, after carrying out filtration treatment, underpressure distillation.

[0033] In the step (d), distillation under reduced pressure is carried out by a rotary evaporator.

[0034] In the step (e), the distilled liquid is washed with an organic solvent.

[0035] In the step (b), the catalyst is an acidic ca...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

No PUM Login to View More

Abstract

The invention discloses a synthetic process of alkene monomers. The synthetic process of alkene monomers comprises the following steps: dissolving raw materials in a solvent, well mixing, reacting to obtain a reaction product mixture, performing reduced-pressure distillation and washing, performing separation and drying to obtain the product. The invention smoothly synthesizes the product, has a high synthetic yield, and reduced production cost; the synthesized alkene monomers can be used to synthesize new polymer scale inhibitors with excellent anti-scaling performance for barium and strontium scale by way of homopolymerization or copolymerization.

Description

technical field [0001] The invention relates to a synthesis process, in particular to a synthesis process of vinyl monomers. Background technique [0002] Formation water is produced during oil extraction, and Ba 2+ 、Sr 2+ , SO 4 2- Anions and cations exist in different formation water and injected water, when Ba 2+ 、Sr 2+ , SO 4 2- After mixing the two water phases, barium sulfate and strontium sulfate scales are easily produced, which block the ground pipelines and rock pores, seriously affecting crude oil production. Because barium and strontium scales are not easy to be dissolved by common acids, once they are formed, they are difficult to remove. Oilfield sites usually use anti-scaling agents to prevent the formation of barium and strontium scales. [0003] The early application of antiscaling agent can be traced back to the 1930s. At that time, the antiscaling agent used was mostly natural products (such as lignin and tannin, etc.), which were not stable in com...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): C07B61/00
Inventor 袁俊海
Owner 袁俊海
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Patsnap Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Patsnap Eureka Blog
Learn More
PatSnap group products