Synthetic process of alkene monomer
A technology for the synthesis of vinyl monomers and synthesis techniques, which is applied in the field of synthesis techniques of vinyl monomers. It can solve the problems of high cost, large dosage, and large chelation stability constant, and achieve high synthesis yields, reduced production costs, and anti-fouling. good performance effect
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[0026] The synthetic technique of the ethylenic monomer that the present invention relates to comprises the following steps:
[0027] (a) raw material is dissolved in solvent, and fully dissolve;
[0028] (b) add catalyst, stir to allow it to fully mix;
[0029] (c) After reacting for a period of time, a reaction product mixture is obtained;
[0030] (d) cooling the reaction product mixture to room temperature, after carrying out vacuum distillation, washing the liquid after distillation;
[0031] (e) separating and drying the washed and distilled liquid to obtain vinyl monomers.
[0032] In said step (d), after the reaction product mixture is cooled to room temperature, after carrying out filtration treatment, underpressure distillation.
[0033] In the step (d), distillation under reduced pressure is carried out by a rotary evaporator.
[0034] In the step (e), the distilled liquid is washed with an organic solvent.
[0035] In the step (b), the catalyst is an acidic ca...
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