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Nano tea saponin environmental-friendly high-efficiency refining agent and preparation method thereof

A nano-tea saponin and refining agent technology, which is applied in textiles, papermaking, and fiber treatment, can solve the problems of poor product quality, long process flow, and low production efficiency, and achieve low cost, wide application, and good product quality Effect

Inactive Publication Date: 2012-06-20
XINYANG HUANYU KNITTING GARMENT
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] With the global low-carbon economy and environmental protection attaching great importance, the traditional pre-treatment process of textile printing and dyeing enterprises has been greatly challenged. The traditional cotton fabric pre-treatment process includes multiple processes such as desizing, scouring, and bleaching. The process is long and Large energy consumption, serious pollution, low production efficiency, poor product quality and other problems

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The present invention is calculated by weight percentage: nano-tea saponin 8%, secondary alkyl sodium sulfonate 8%, C12-14 alkyl polyglycoside 7%, isomeric C13 alcohol polyoxyethylene ether 7%, carboxymethyl cellulose 1%, chelating dispersant HW-508 0.2%, 4A zeolite 2%, sodium carbonate 6.5%, defoamer 0.2%, ion water 60.1%, among them, first add ion water 60.1% in the reaction kettle, in Add 8% sodium secondary alkyl sulfonate (SAS60) at 40°C, stir well (40 minutes), then add 7% C12-C14 alkyl polyglycoside and 7% isomeric C13 alcohol polyoxyethylene ether, Continue to stir for 45 minutes, then gradually increase the temperature to 65°C, add 8% nano-tea saponin (particle size 5-200nm, saponin ≥ 97%) to the above mixture, stir well for 100 minutes, then cool down to room temperature, and Add 1% carboxymethyl cellulose, 2% 4A zeolite, and 0.2% chelating dispersant HW-508 into the reactor, stir evenly for 40 minutes, then add 6.5% sodium carbonate into the reactor and stir ...

Embodiment 2

[0027] The present invention can also be calculated by the following percentages by weight in practice: 10% of nano-tea saponin, 9% of secondary alkyl sodium sulfonate, 8% of C12-14 alkyl polyglycoside, 8% of isomerized C13 alcohol polyoxyethylene ether, Carboxymethyl cellulose 1.5%, chelating dispersant HW-508 0.5%, 4A zeolite 2.5%, sodium carbonate 4.5%, defoamer 0.3%, ionized water 55.7%, among them, add ion in the reaction kettle Water 55.7%, add 9% sodium secondary alkyl sulfonate (SAS60), heat up to 40°C and stir evenly for 50 minutes, then add 8% C12-14 alkyl polyglycoside and 8% isomeric C13 alcohol polyoxygen Vinyl ether, continue to stir for 60 minutes, then gradually increase the temperature to 70 ° C, add 10% nano-tea saponin (particle size 5-200nm, saponin ≥ 97%), fully stir for 120 minutes, then cool down to room temperature, 1.5 % carboxymethyl cellulose, 2.5% 4A zeolite, 0.5% chelating dispersant HW-508 were added to the reactor, stirred for 60 minutes, then 4....

Embodiment 3

[0029]The present invention is calculated by weight percentage: 12% of nano-tea saponin, 10% of sodium secondary alkyl sulfonate, 9% of C12-14 alkyl polyglycoside, 10% of isomeric C13 alcohol polyoxyethylene ether, carboxymethyl cellulose 2%, chelating dispersant HW-508 0.8%, 4A zeolite 3%, sodium carbonate 3%, defoamer 0.4%, ionized water 49.8%, among them, add ionized water 49.8% in the reaction kettle first, add 10% sodium secondary alkyl sulfonate (SAS60), heat up to 40°C and stir evenly for 60 minutes, then add 9% C12-14 alkyl polyglycoside and 10% isomeric C13 alcohol polyoxyethylene ether, continue stirring evenly 50 minutes, then gradually increase the temperature to 70°C, add 12% nano-tea saponin (particle size 5-200nm, saponin ≥ 97%) to the above mixture, stir for 150 minutes, then lower to room temperature, add 2% carboxylated Add methylcellulose, 3% 4A zeolite, and 0.8% chelating dispersant HW-508 into the reaction kettle, stir for 50 minutes, then add 3% sodium ca...

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Abstract

The invention relates to a nano tea saponin environmental-friendly high-efficiency refining agent and a preparation method thereof and can effectively solve the problem of preparing the refining agent for textile pretreatment by utilizing nano tea saponin. In the method, the nano tea saponin environmental-friendly high-efficiency refining agent is prepared from the following components in percentage by weight: 7 to 15 percent of nano tea saponin, 7 to 12 percent of secondary alkane sulphonate sodium, 7 to 12 percent of C12-C14 alkyl polyglucosides, 7 to 12 percent of heterogeneous C13 alcoholethoxylates, 1 to 5 percent of carboxymethylcellulose, 0.1 to 2 percent of chelating disperse agent HW-508, 1 to 6 percent of 4A zeolite, 3 to 8 percent of sodium carbonate, 0.1 to 1 percent of antifoaming agent and the balance of ionized water, wherein the method comprises the following steps: adding the ionized water and secondary alkane sulphonate sodium into a reaction kettle, stirring and uniformly mixing; then adding the C12-C14 alkyl polyglucosides and the heterogeneous C13 alcohol ethoxylates, stirring and uniformly mixing; warming, adding nano tea saponin, stirring and uniformly mixing; reducing the temperature, adding the carboxymethylcellulose, the 4A zeolite and the chelating disperse agent HW-508, stirring and uniformly mixing; adding the sodium carbonate and regulating the pH value; and adding the antifoaming agent and uniformly mixing to obtain the nano tea saponin environmental-friendly high-efficiency refining agent. The nano tea saponin environmental-friendly high-efficiency refining agent has scientific and reasonable components, simple method, low cost, high quality and wide application and is efficient, environmental-friendly and energy-saving.

Description

technical field [0001] The invention relates to a refining agent in the field of textile chemistry, in particular to a nano-tea saponin environment-friendly and high-efficiency refining agent and a preparation method thereof. Background technique [0002] With the global low-carbon economy and environmental protection attaching great importance, the traditional pre-treatment process of textile printing and dyeing enterprises has been greatly challenged. The traditional cotton fabric pre-treatment process includes multiple processes such as desizing, scouring, and bleaching. The process is long and Large energy consumption, serious pollution, low production efficiency, poor product quality and other problems. In order to meet the needs of global green barriers and environmental protection and energy saving, the traditional textile pretreatment process is gradually replaced by a new short-process descouring and bleaching one-step process. Therefore, it is very important to dev...

Claims

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Application Information

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IPC IPC(8): D06M13/224D06M13/256D06M15/53D06M15/09D06M11/76D06M11/79
Inventor 赵鑫荣
Owner XINYANG HUANYU KNITTING GARMENT
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