Binder for lithium secondary battery, negative electrode for lithium secondary battery, lithium secondary battery, binder precursor solution for lithium secondary battery, and method for manufacturing negative electrode for lithium secondary battery
A lithium secondary battery and precursor solution technology, applied in battery electrodes, lithium storage batteries, adhesives, etc., can solve the problem of reduced charge-discharge cycle characteristics of lithium secondary batteries, large volume changes of negative electrode active materials, negative electrode active materials and negative electrode active materials. Layer detachment and other problems, to achieve the effect of excellent charge-discharge cycle characteristics
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Embodiment 1
[0077] In Example 1, a battery A1 having substantially the same configuration as the lithium secondary battery 1 of the above-described embodiment was produced in the following manner.
[0078] [Production of Negative Electrode]
[0079] (1) Preparation of negative electrode active material
[0080] First, polysilicon particles are introduced into the fluidized bed with an internal temperature of 800°C, and at the same time, monosilane (SiH 4 ), thereby producing granular polycrystalline silicon, and then pulverizing the granular polycrystalline silicon using a jet mill, and then classifying in a classifier to produce polycrystalline silicon powder (negative electrode active material). The median diameter of the polycrystalline silicon powder was 10 μm. The crystallite size of the polycrystalline silicon powder is 44nm.
[0081] In addition, the median diameter is a 50% cumulative volume particle diameter in particle size distribution measurement by a laser diffraction meth...
Embodiment 2
[0106] In the preparation of the binder precursor solution, (3,3',4,4'-benzophenone tetracarboxylic dianhydride):(m-phenylenediamine):(3-aminopropyltriethoxy A battery A2 was fabricated in the same manner as in Example 1 above, except that the molar ratio was 100:100:5.
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