Measuring method of iron
A measurement method, lithium iron phosphate technology, applied in the field of detection, can solve the problems of expensive instruments and consumables, high cost, cumbersome testing process, etc.
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Embodiment 1
[0040] Instruments and medicines: 10mL colorimetric tube, 100mL polyethylene bottle (with inner lining), potassium thiocyanide (analytical pure), nitric acid (analytical pure), 1000ppm Fe 3+ Iron standard solution (excellent grade)
[0041] Determination steps:
[0042] Configuration of potassium thiocyanate solution: Weigh 25 g of potassium thiocyanide, add pure water to dissolve, and set the volume to 100 mL to obtain a potassium thiocyanide solution with a mass volume concentration of 25% g / ml.
[0043] Sample pretreatment: take lithium iron phosphate and bake at a high temperature of 120° C. for 4 hours.
[0044] Test the dissolution of iron at room temperature: Weigh 5.0000g of lithium iron phosphate material, pipette 50mL of electrolyte solution and add it, shake it well and store it sealed for 2 days, filter it with qualitative double-layer filter paper, put the filtrate in a plastic beaker and label it, and get First test solution.
[0045] High-temperature test for...
Embodiment 2~4
[0050] Using the detection method in Example 1, respectively, the amount of iron dissolution was measured for lithium iron phosphate produced by different manufacturers.
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