Acetate solvent based diesel oil pour point depressant, preparation method and application thereof

A diesel pour point depressant, solvent-based technology, used in the petroleum industry, fuel additives, liquid carbon-containing fuels, etc., can solve the problem that high-waxy diesel has no improvement effect, strong dependence on diesel components, and poor wax crystal cluster dispersion. problem, to achieve the effect of improving low temperature fluidity, simple preparation method and improving dispersion effect

Inactive Publication Date: 2012-08-15
SHANGHAI INST OF TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

From the perspective of practical application effect, the main problem faced by diesel pour point depressants is that the developed varieties have strong dependence on diesel components and poor susceptibility to different components of diesel, especially for high waxy diesel, which has almost no improvement effect. Its application is very limited
From the experiments and the structural analysis of the pour point depressant, it is believed that the poor dispersibility of the pour point depressant to the wax crystal clusters that appear at low temperature of diesel oil is the main reason for its poor sensitivity

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] An acetate solvent type diesel oil point depressant composition, its raw materials are calculated by mass percentage, and its composition and content are as follows:

[0028] Ethyl acetate 10%

[0029] Propyl acetate 10%

[0030] Butyl acetate 40%

[0031] Amyl acetate 20%

[0032] Diesel pour point depressant 10%;

[0033] Wherein, the diesel pour point depressant used is polymethacrylate (PMA) diesel pour point depressant 10-310.

[0034] The preparation method of above-mentioned a kind of acetate solvent type diesel oil point depressant, comprises the following steps:

[0035] After mixing the raw materials, stir in a constant temperature water bath at 50°C, control the rotation speed at 120r / min, and stir for 30min to obtain an acetate-based solvent-based diesel pour point depressant composition 1.

[0036] The application of the above-mentioned acetate-based solvent-based diesel pour point depressant composition 1 in diesel oil pour point depressant, that is, ...

Embodiment 2

[0038] An acetate solvent type diesel oil point depressant composition, its raw materials are calculated by mass percentage, and its composition and content are as follows:

[0039] Ethyl acetate 10%

[0040] Propyl acetate 20%

[0041] Butyl acetate 30%

[0042] Amyl acetate 20%

[0043] Diesel pour point depressant 20%;

[0044] Wherein, the diesel pour point depressant used is polymethacrylate (PMA) diesel pour point depressant 10-310.

[0045] After mixing the raw materials, stir in a constant temperature water bath at 50°C, control the rotation speed at 120r / min, and stir for 30min to obtain an acetate-based solvent-based diesel pour point depressant composition 2.

[0046] The application of the above-mentioned acetate-based solvent-based diesel pour point depressant composition 2 in diesel oil pour point depressant, that is, the acetate-based solvent-based diesel pour point depressant composition 2 calculated by mass ratio: commercially available 0# diesel oil is 1 ...

Embodiment 3

[0048] An acetate solvent type diesel oil point depressant composition, its raw materials are calculated by mass percentage, and its composition and content are as follows:

[0049] Ethyl acetate 10%

[0050] Propyl acetate 20%

[0051] Butyl acetate 20%

[0052] Amyl acetate 20%

[0053] Diesel pour point depressant 30%;

[0054] Wherein, the diesel pour point depressant used is polymethacrylate (PMA) diesel pour point depressant 10-310.

[0055]After mixing the raw materials, stir in a constant temperature water bath at 50°C, control the rotation speed at 120r / min, and stir for 30min to obtain an acetate-based solvent-based diesel pour point depressant composition 3.

[0056] The application of the above-mentioned acetate-based solvent-based diesel pour point depressant composition 3 in diesel oil pour point depressant, that is, the acetate-based solvent-based diesel pour point depressant composition 3 calculated by mass ratio: commercially available 0# diesel oil is 1 ...

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PUM

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Abstract

The invention discloses an acetate solvent based diesel oil pour point depressant composition, a preparation method and an application of the acetate solvent based diesel oil pour point depressant. The acetate solvent based diesel oil pour point depressant composition comprises the components by mass percent: 0-10% of ethyl acetate, 0-20% of propyl acetate, 20-40% of butyl acetate, 0-20% of amyl acetate and 10-30% of diesel oil pour point depressant. The preparation method comprises the steps of: mixing all the raw materials and stirring in thermostatic water bath; and controlling the rotating speed to be 120r/min to obtain the acetate solvent based diesel oil pour point depressant 30minutes later. The acetate solvent based diesel oil pour point depressant composition improves the dispersive action of the diesel oil pour point depressant for wax crystals at the low temperature, and improves the low-temperature fluidity of oil products; and the acetate solvent based diesel oil pour point depressant composition can be added into commercially available 0-model diesel oil, so that the cold filter plugging point is reduced by 5-11 DEG C, and the condensation point is reduced by 6-10 DEG C.

Description

technical field [0001] The invention relates to a pour point depressant and a preparation method thereof, in particular to an acetate-based solvent-based diesel pour point depressant for diesel pour point depressant, a preparation method and application thereof. Background technique [0002] Diesel pour point depressant is an additive that can significantly reduce the freezing point and cold filter point of diesel and improve the low temperature flow performance of diesel when added in a small amount. It mainly improves the low temperature flow properties of diesel through eutectic, adsorption, solubilization or nucleation. The research on diesel oil pour point depressant is of great significance to increase the output of diesel oil, save kerosene, increase the ratio of diesel to gasoline and improve the economic benefits of refineries. At present, in order to obtain a better cooling filter point reduction effect, domestic and foreign mainly focus on the research on the co...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10L1/19C10L10/14
Inventor 韩生曹磊昌刘天齐李然孙揭阳郁平朱贤王爱民
Owner SHANGHAI INST OF TECH
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