Sibiraea effective-part extract, preparation method and use thereof
A technology of effective parts and extracts, applied in the field of willow tea effective parts extract and its preparation, can solve the problems of deep color, peculiar smell and high cost
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Embodiment 1
[0023] Example 1 Preparation of effective part extract of willow tea
[0024]Grind 10 kg of dry willow tea, then extract by heating 100 liters of 1% sodium bicarbonate aqueous solution under reflux for 2 hours, filter the insoluble residue, wash and degrease the obtained water extract with 50 liters of petroleum ether, and then concentrate to Dry, and make 1.3 kilograms of willow tea water extraction paste; 6 kilograms of ethanol heating reflux extracts the above-mentioned pulverized willow tea water extraction paste for 2 hours, obtains 0.54 kilograms of ethanol extracts after the ethanol extract is concentrated to dryness; Analysis, the consumption of adsorbent activated carbon is 1 kilogram, is that 20% ethanol aqueous solution is eluted as eluent with volume concentration, uses silica gel thin-layer chromatography to detect eluent and elution process, and spraying volume concentration is 10% sulfuric acid Methanol solution is used as a chromogen, and 110 o Heating at C fo...
Embodiment 2
[0025] Example 2 Safety inspection of the effective part extract of willow tea
[0026] According to the "Examination Method for Abnormal Toxicity" of the third part of the Chinese Pharmacopoeia in 2010: each drug has 5 healthy mice, and the test product is the effective part extract of willow tea prepared in Example 1, intraperitoneal injection, according to the conventional acute toxicity test Testing was carried out, and the result was normal feeding, and no death was seen within 7 days of observation.
Embodiment 3
[0027] Example 3 Health food with effective part extract of willow tea as effective additive
[0028] The effective part extract of willow tea prepared in Example 1 can be included in foods such as bread, noodles, cakes, biscuits, milk, yogurt and beverages or mineral water in the form of additives, condiments such as soy sauce, oils such as rapeseed oil, sesame oil, tea oil , corn oil and peanut oil, wine such as rice wine, beer, liquor and so on. The dosage of the additive is equivalent to 0.01-10% of the weight of the food.
[0029]
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