Preparation method for indium oxide sequential nano mesoporous materials doping with metal
A nano-mesoporous material, indium oxide technology, applied in chemical instruments and methods, nanotechnology for materials and surface science, nanotechnology, etc., can solve problems such as inappropriate doping of various metals, and achieve broadened uses and shapes Consistent, low-equipment-required results
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[0034] Example 1: Preparation of Zn doped In 2 O 3 Ordered Nano Mesoporous Materials
[0035] 10g surfactant P123, 3g In(NO 3 ) 3 ·4.5H 2 O, 0.291g Zn(NO 3 ) 2 ·6H 2 O, 50g ethanol is stirred until it is completely dissolved, then add 25g TEOS, stir for 10min, add 3g 1mol / L HCl and stir for 10min, transfer to a porcelain boat and place in the air for 72h; spread 3mm thick paraffin on the surface of the sample, oil bath Heat at 60°C for 24h, wipe off the paraffin on the surface of the sample, and then roast in a muffle furnace (heating rate 3°C / min) at 500°C for 8h; add 40ml of 2mol / L NaOH solution to the sample and stir for 2h, then centrifuge to remove the upper layer Clear liquid, repeat the operation 3 times, then wash twice with water and ethanol, and dry in air to obtain In 2 O 3 Ordered nano mesoporous materials.
[0036] After structural characterization, the obtained Zn doped In 2 O 3 Ordered nanometer mesoporous materials have a pore diameter of 2.8nm and a specific surfac...
Example Embodiment
[0037] Example 2. Preparation of Cu-doped In 2 O 3 Ordered Nano Mesoporous Materials
[0038] 10g surfactant P123, 3g In(NO 3 ) 3 ·4.5H 2 O, 0.236gCu(NO 3 ) 2 ·3H 2 O, 50g ethanol is stirred until it is completely dissolved, then add 25g TEOS, stir for 10min, add 3g 1mol / L hydrochloric acid and stir for 10min, transfer to a porcelain boat and place in the air for 72h; spread 3mm thick paraffin on the surface of the sample, oil bath Heat at 50°C for 30h, wipe off the paraffin on the surface of the sample, and then roast at 500°C for 8h in a muffle furnace (heating rate 1°C / min); add 30ml of 3mol / L NaOH solution to the sample and stir for 2h, then centrifuge to remove the upper layer Clear liquid, repeat the operation 3 times, then wash twice with water and ethanol, and dry in the air to obtain In 2 O 3 Ordered nano mesoporous materials.
[0039] After structural characterization, the Cu doped In 2 O 3 The ordered nano mesoporous material has a regular pore diameter of 2.9nm and a sp...
Example Embodiment
[0040] Example 3: Preparation of Mg doped In 2 O 3 Ordered nano mesoporous materials
[0041] 10g surfactant P123, 3g In(NO 3 ) 3 ·4.5H 2 O, 0.25g Mg(NO 3 ) 2 ·6H 2 O, 50g ethanol is stirred until it is completely dissolved, then add 25g TEOS, stir for 10min, add 3g 1mol / L HCl and stir for 10min, transfer to a porcelain boat and place in the air for 72h; spread 3mm thick paraffin on the surface of the sample, oil bath Heat at 60°C for 24h, wipe off the paraffin on the surface of the sample, then calcinate at 500°C for 7h in a muffle furnace (heating rate 5°C / min); add 60ml of 1mol / L NaOH solution to the sample and stir for 2h, then centrifuge to remove the upper layer Clear liquid, repeat the operation 5 times, then wash twice with water and ethanol, and dry in the air to obtain In 2 O 3 Ordered nano mesoporous materials.
[0042] After structural characterization, the obtained Mg doped In 2 O 3 The ordered nano mesoporous material has a pore size of 4.1nm and regular pores, with a...
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