Coloring cured resin composite
A curable resin and composition technology, applied in coatings, instruments, and photosensitive materials used in optomechanical equipment, etc., can solve the problems of dry matter, drying of colored curable resin compositions, etc., and achieve inhibition of clogging, re- Excellent solubility and the effect of suppressing defective products
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment
[0318] The present invention will be further described in detail through examples below, but the present invention is not limited by these examples. In Examples and Comparative Examples, % and parts indicating content or usage-amount are based on mass unless otherwise specified.
Synthetic example 1
[0320]
[0321] In a flask with a condensing tube and a stirring device, 15 parts of a mixture of a compound represented by formula (A0-1) and a compound represented by formula (A0-2) (manufactured by Zhongwaihuacheng), 150 parts of chloroform and N, N- To 8.9 parts of dimethylformamide, 10.9 parts of thionyl chloride were added dropwise while maintaining the temperature below 20°C under stirring. After completion of the dropwise addition, the temperature was raised to 50°C, and the reaction was maintained at this temperature for 5 hours, and then cooled to 20°C. While maintaining the cooled reaction solution at 20° C. or lower with stirring, a mixed solution of 12.5 parts of 2-ethylhexylamine and 22.1 parts of triethylamine was added dropwise. Then, stirring was carried out at this temperature for 5 hours to make it react. Then, after distilling off the solvent from the obtained reaction mixture with a rotary evaporator, a small amount of methanol was added and vigorously ...
Synthetic example 2
[0327]
[0328] In a 1L flask with a stirrer, a thermometer, a reflux condenser and a dropping funnel, flow nitrogen gas at 0.02L / min to obtain a nitrogen atmosphere, add 305 parts of propylene glycol monomethyl ether acetate, and heat to 70°C. Then dissolve in 60 parts of methacrylic acid, 3,4-epoxy tricyclic [5.2.1.0 2.6 ] decyl acrylate (mix the compound represented by the following formula (B-1-1) and the compound represented by formula (B-1-2) at a molar ratio of 50:50.) 240 parts, and propylene glycol monomethyl 140 parts of ether acetate was used to prepare a solution, and the solution was dropped into a flask kept at 70° C. over 4 hours using a dropping funnel. On the other hand, using another dropping funnel, a solution obtained by dissolving 30 parts of the polymerization initiator 2,2'-azobis(2,4-dimethylvaleronitrile) in 225 parts of ethyl lactate was prepared over 4 hours. Add dropwise to the flask. After the solution of the polymerization initiator was added...
PUM
Property | Measurement | Unit |
---|---|---|
boiling point | aaaaa | aaaaa |
acid value | aaaaa | aaaaa |
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com