Solar polycrystalline silicon purification equipment employing directional solidification metallurgical method
A technology of directional solidification and metallurgy, which is applied in self-solidification, polycrystalline material growth, crystal growth, etc., can solve the problems of small capacity, low yield, poor product quality homogeneity, etc., and achieve low cost and long service life , the effect of good directional solidification speed
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example 1
[0070] 1. Automatic temperature control system data writing
[0071] Set the temperature control curve of the top thermocouple as:
[0072] 1430℃-------Insulation-----1h
[0073] 1430℃-------1428℃-----5h
[0074] 1428℃-------1426℃-----5h
[0075] 1426℃-------1424℃-----5h
[0076] 1424℃-------1422℃-----5h
[0077] 1422℃-------1420℃-----5h
[0078] Naturally cool down to 600°C when power is off
[0079] The temperature control curve of the bottom thermocouple is:
[0080] 1420℃-------Insulation-----1h
[0081] 1420℃-------1419℃-----2h
[0082] 1419℃-------1418℃-----1h
[0083] 1418℃-------1417℃-----1h
[0084] 1417℃-----1380℃-----20h
[0085] Natural cooling to 500°C when power off
[0086] 2. The inner size of graphite ingot mold is 1500*1200*400mm
[0087] 3. The capacity of intermediate frequency furnace is 1500kg, graphite crucible.
[0088] 4. The silicon material adopts metal silicon with a P value of about 1ppmw and a total amount of metal elements below 100...
example 2
[0093] 1. Automatic temperature control system data writing
[0094] Set the temperature control curve of the top thermocouple as:
[0095] 1450℃-------Insulation-----1h
[0096] 1450℃-------1430℃-----2h
[0097] 1430℃-------1428℃-----4h
[0098] 1428℃-------1426℃-----3h
[0099] 1426℃-------1424℃-----2h
[0100] 1424℃-------1422℃-----1h
[0101] 1422℃-------1420℃---15h
[0102] Naturally cool down to 600°C when power is off
[0103] The temperature control curve of the bottom thermocouple is:
[0104] 1420℃-------Insulation-----1h
[0105] 1420℃-------1419℃-----3h
[0106] 1419℃-------1418℃-----2h
[0107] 1418℃-------1417℃-----0.5h
[0108] 1417℃-----1380℃-----19h
[0109] Natural cooling to 500°C when power off
[0110] 2. The inner size of graphite ingot mold is 1500*1200*400mm
[0111] 3. The capacity of intermediate frequency furnace is 1500kg, graphite crucible.
[0112] 4. The silicon material adopts metal silicon with a P value of about 1ppmw and a tota...
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