Complex formulation comprising aspirin coated with barrier containing hydrophobic additive, and hmg-coa reductase inhibitor
A technology of reductase inhibitor and hydrophobic additive, applied in the field of compound preparation, can solve problems such as adverse side effects, occurrence of gastric ulcer or gastric bleeding, adverse interaction and the like
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Embodiment 1
[0039] Example 1: Preparation of Aspirin Pellets and Granules
[0040] Preparation of aspirin pellets
[0041] According to Table 1, aspirin (Spectrum Chemical, US), hydroxypropyl methylcellulose (HPMC; Shinetsu, Japan), citric acid, and talc (Nippon talc, Japan) were dissolved and dispersed in a mixed solution of water and ethanol to A coating solution containing aspirin was prepared. The coating solution was sprayed while fluidizing microcrystalline spherical beads (cellet; Pharmatrans) using a fluidized bed sprayer (NQ-125, Fuji Paudal, Japan) to prepare aspirin pellets.
[0042] Preparation of aspirin granules
[0043] According to Table 1, aspirin, microcrystalline cellulose (Avicel) (FMC biopolymer, US), citric acid and mannitol were mixed and kneaded using hydroxypropylmethylcellulose (HPC) dissolved in water and ethanol, followed by Extruded using an extruder (MG-55, Dalton, Japan). Then, the extruded product was spheronized using a spheronizer (Q-230T, Dal...
Embodiment 2 to 7
[0046] Examples 2 to 7: Coating with barrier agent containing hydrophobic additive (1)
[0047] According to Table 2, the aspirin pellets or granules of Example 1 were coated with a barrier agent containing hydrophobic additives of various compositions. Specifically, HPMC, acetylated monoglyceride ( Kerry bio-sCience, US), talc, titanium dioxide (TiO 2 ) and hydrophobic additives (carnauba wax or ethylcellulose (EC, Colorcon)) were dissolved and dispersed in a mixed solution of water and ethanol to prepare a barrier agent coating solution. Then, each coating solution was sprayed while fluidizing aspirin pellets or granules (cellet; Pharmatrans) using a fluidized bed spraying machine (NQ-125, Fuji Paudal, Japan) to prepare aspirin pellets coated with a barrier agent. grain.
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Embodiment 8 and comparative Embodiment 4
[0054] Example 8 and Comparative Example 4: Coating with barrier agent containing hydrophobic additive (2)
[0055] According to the same method as in Example 2 to Example 7, the pellets of Example and Comparative Example 3 were coated with a barrier agent containing a hydrophobic additive as shown in Table 4, respectively.
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