Monomer casting (MC) nylon polishing abrasive grain used in roller polishing machine and preparation method of MC nylon polishing abrasive grain
A barrel polishing, polishing and grinding technology, applied in chemical instruments and methods, polishing compositions containing abrasives, other chemical processes, etc., can solve the problems of long time, difficult to remove and separate, affect the use effect, etc., and achieve easy separation. , excellent polishing effect, excellent wear resistance and polishing efficiency
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Embodiment
[0022] According to its mass percentage: caprolactam monomer (MC nylon) 70%, polyethylene wax 2%, artificial diamond powder with particle size W0.5 / 1 20%, cerium oxide 8%;
[0023] Put the caprolactam monomer into a dry and clean reaction vessel, heat and melt it, add artificial diamond micropowder and cerium oxide powder, stir it vigorously, disperse it ultrasonically, add polyethylene wax, and pump it under a vacuum degree greater than 0.1 MPa and a temperature of 130°C. Vacuum dehydration is complete, then release the vacuum, add 0.5% (calculated by the mass of caprolactam) NaOH, continue to vacuumize and dehydrate completely, release the vacuum, adjust the solution to 100 ° C, add 0.5% (calculated by the mass of caprolactam) toluene diisocyanate (TDI ), stirred evenly, cast into a preheated tetrafluoroethylene mold, reacted for 30 minutes, cooled naturally to suffocating temperature, and demolded to obtain MC nylon diamond polishing abrasive grains.
Embodiment 2
[0025] According to its mass percentage: caprolactam monomer (MC nylon) 80%, polypropylene wax 3%, silicon carbide powder 15%, cerium oxide 2%, silicon carbide powder particle size W5;
[0026] Put the caprolactam monomer into a dry and clean reaction vessel, heat and melt it, add abrasives and cerium oxide powder, stir it vigorously, disperse it ultrasonically, add polypropylene wax, and vacuum dehydrate it at a vacuum degree greater than 0.1 MPa and a temperature of 130°C complete, then remove the vacuum, add 0.5% (calculated by the mass of caprolactam) NaOH, continue vacuuming and dehydration completely, release the vacuum, adjust the solution to 100 ° C, add 0.5% (calculated by the mass of caprolactam) toluene diisocyanate (TDI), Stir evenly, cast into a preheated tetrafluoroethylene mold, react for 30 minutes, cool naturally to suffocating temperature, and demold to obtain MC nylon silicon carbide polishing abrasive grains.
Embodiment 3
[0028] According to its mass percentage: caprolactam monomer (MC nylon) 90%, polyethylene wax 5%, nano-diamond 5%.
[0029] Put the caprolactam monomer into a dry and clean reaction vessel, heat and melt it, add nano-diamonds, stir vigorously, add polyethylene wax, vacuumize and dehydrate completely at a vacuum degree greater than 0.1 MPa and a temperature of 130°C, and then release the vacuum. Add 0.5% (calculated by the mass of caprolactam) NaOH, continue vacuuming to complete the dehydration, release the vacuum, adjust the solution to 100°C, add 0.5% (calculated by the mass of caprolactam) toluene diisocyanate (TDI), stir evenly, and cast to the pre- In a hot tetrafluoroethylene mold, react for 30 minutes, cool naturally to suffocation temperature, and demold to obtain MC nylon nano-diamond polishing abrasive grains.
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