Wolfberry extract containing wolfberry acid and preparation method thereof
A technology of wolfberry extract and wolfberry acid, which is applied in the preparation of sugar derivatives, chemical instruments and methods, sugar derivatives, etc., can solve problems such as insufficient guarantee of the quality of deep-processed products of wolfberry, and achieve the effect of great application value and social benefit.
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Embodiment 1
[0028] Weigh 10 kilograms of dried wolfberry fruit produced in Ningxia, rinse with reverse osmosis drinking pure water to remove floating dust. Use reverse osmosis drinking pure water to extract twice, the dosage is 80KG each time, each static extraction is 2 hours, and the extraction temperature is 80°C. The feed liquid obtained by leaching is filtered in situ. The combined extracts were filtered with a 0.1 μm fine filter membrane. The filtrate is treated with a 10000D ultrafiltration membrane to obtain two parts: the retentate after ultrafiltration and the pass through after ultrafiltration. The passing liquid after ultrafiltration is added and treated with a column volume of 1 molar sodium hydroxide solution, and then washed with pure drinking water by reverse osmosis to neutral OH - The column packed with ZB-2 strong basic anion exchange fiber is added at a flow rate of 1 column volume / hour. After adding the feed liquid, use reverse osmosis drinking pure water to wash t...
Embodiment 2
[0032]Weigh 10 kilograms of dried wolfberry fruit produced in Ningxia, rinse with reverse osmosis drinking pure water to remove floating dust. Extract twice with reverse osmosis drinking pure water, the dosage is 120KG each time, each static extraction is 1.5 hours, and the extraction temperature is 50°C. The feed liquid obtained by leaching is obtained by in-situ filtration. The combined extracts were filtered with a plate and frame filter and 0.1 kg of talcum powder was used as a filter aid. The filtrate is treated with a 5000D ultrafiltration membrane to obtain two parts: the retentate after ultrafiltration and the pass through solution after ultrafiltration. The passing liquid after ultrafiltration was added to the column filled with ZB-2 strongly basic anion exchange fiber treated into OHˉ type (treated according to the method of Example 1), and the flow rate was 1 column volume / hour. After adding the feed liquid, use reverse osmosis drinking pure water to wash the ion ...
Embodiment 3
[0034] Weigh 10 kilograms of dried wolfberry fruit produced in Ningxia, rinse with reverse osmosis drinking pure water to remove floating dust. Use reverse osmosis drinking pure water to extract twice, the dosage is 150KG each time, each static extraction is 3 hours, and the extraction temperature is 30°C. The feed liquid obtained by leaching is obtained by in-situ filtration. The combined soaking extracts were filtered with a 0.1 μm fine filter membrane. The filtrate is treated with an 8000D ultrafiltration membrane to obtain two parts: the retentate after ultrafiltration and the pass through after ultrafiltration. The passing liquid after ultrafiltration was added to the column filled with ZB-2 strongly basic anion exchange fiber treated into OHˉ type (treated according to the method of Example 1), and the flow rate was 1 column volume / hour. After adding the feed liquid, use reverse osmosis drinking pure water to wash the ion exchange column until the effluent is clear and...
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