Calcium tablet using deep-sea fish bone as raw material and preparation method thereof
A deep-sea fish and fish bone technology, applied in the field of health care products, can solve the problems of strong alkalinity of calcium source, failure of effective supplementation of calcium element, limited solubility of calcium element, etc.
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Embodiment 1
[0023] (1) Weigh a certain amount of fish bones, wash them with clean water, put them in a cooking pot, add water and cook for 1 hour, remove the fish bones and place them in a drying oven at 160°C to dry until the water content is about 10 (wt)%. Then put it in a pulverizer for pulverization, and then pulverize it to a particle size of more than 300 mesh by using an ultrafine pulverization grade.
[0024] (2) Fishbone powder and 1mol / L sodium hydroxide solution are mixed according to the ratio of 1:5 (mass ratio), soaked for 24 hours, filtered, and soaked with 60 (wt)% ethanol solution after the fishbone powder is cleaned to neutrality (mass ratio 1:5) for 18 hours, filtered, washed with distilled water to remove alcohol, and dried until the water content was about 10 (wt)%.
[0025] (3) Fishbone powder and distilled water are mixed according to the ratio of 1:1 (mass ratio) and placed in a container, and papain and flavor enzymes with 2% of the quality of fishbone powder are...
Embodiment 2
[0029] (1) Weigh a certain amount of fish bones, wash them with clean water, put them in a cooking pot, add water and cook for 1 hour, remove the fish bones and place them in a drying oven at 160°C to dry until the water content is about 10 (wt)%. Then put it in a pulverizer for pulverization, and then pulverize it to a particle size of more than 300 mesh by using an ultrafine pulverization grade.
[0030] (2) Fishbone powder and 1mol / L sodium hydroxide solution were mixed according to the ratio of 1:5 (mass ratio), soaked for 30 hours, filtered, washed with 60 (wt)% ethanol solution after the fishbone powder was washed to neutrality (mass ratio 1:5) for 15 hours, filtered, washed with distilled water to remove alcohol, and dried until the water content was about 10 (wt)%.
[0031] (3) Fishbone powder and distilled water are mixed according to the ratio of 1:1 (mass ratio) and placed in a container, and papain and flavor enzymes with 2% of the quality of fishbone powder are ad...
Embodiment 3
[0035] (1) Weigh a certain amount of fish bones, wash them with clean water, put them in a cooking pot, add water and cook for 1 hour, remove the fish bones and place them in a drying oven at 160°C to dry until the water content is about 10 (wt)%. Then put it in a pulverizer for pulverization, and then pulverize it to a particle size of more than 300 mesh by using an ultrafine pulverization grade.
[0036] (2) Fishbone powder and 1mol / L sodium hydroxide solution are mixed according to the ratio of 1:5 (mass ratio), soaked for 36 hours, filtered, and soaked with 60 (wt)% ethanol solution after the fishbone powder is washed to neutrality (mass ratio 1:5) for 12 hours, filtered, washed with distilled water to remove alcohol, and dried until the water content was about 10 (wt)%.
[0037] (3) Fishbone powder and distilled water are mixed according to the ratio of 1:1 (mass ratio) and placed in a container, and papain and flavor enzymes with 3% of the quality of fishbone powder are ...
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