Synchronous preparation method of four effective parts in medicine pair of common anemarrhena rhizome and amur corktree bark and application thereof
A technology of effective parts and Cortex Phellodendri, which is applied in the field of simultaneous preparation of four effective parts of Anemarrhena Phellodendri in medicine pairs, can solve the problems of few studies on Anemarrhena Phellodendri, and achieve the effects of easy industrial production, avoiding waste of resources and improving efficiency.
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Embodiment 1
[0054] A method for synchronously preparing four effective parts of the Anemarrhena Phellodendron herb pair. The four effective parts are respectively total polysaccharide extract, total saponin extract, total flavonoid extract, and total alkaloid extract. The simultaneous preparation method includes Follow the steps below:
[0055] (1) Grind Anemarrhena anemarrhena and Cortex Phellodendri (50g each) with a weight ratio of 1:1 to 10-120 mesh, soak in ethanol with a volume concentration of 65% for 2-3 hours, and reflux (control the temperature at 80-100°C) Extract 3 times, then reflux with 40% ethanol (temperature controlled at 80-100°C) to extract 3 times, and combine the extracts; the amount of ethanol used for each extraction is 6-10% of the total weight of Anemarrhena and Cortex Phellodendri times, each extraction time is 1-2h;
[0056] (2) Filter the extract obtained in step (1) with a filter bag of 300-400 mesh, and pass the filtrate through the series connection of PIPO...
Embodiment 2
[0066] A method for synchronously preparing four effective parts of the Anemarrhena Phellodendron herb pair. The four effective parts are respectively total polysaccharide extract, total saponin extract, total flavonoid extract, and total alkaloid extract. The simultaneous preparation method includes Follow the steps below:
[0067] (1) Grind Anemarrhena anemarrhena and Cortex Phellodendri (500g and 400g respectively) with a weight ratio of 1:0.8 to 10-120 mesh, soak in ethanol with a volume concentration of 75% for 2-3h, and reflux (the temperature is controlled at 80- 100°C) for 5 extractions, then reflux with 60% ethanol (temperature controlled at 80-100°C) for 4 extractions, and combine the extracts; the amount of ethanol used for each extraction is the total weight of Anemarrhena and Cortex 6-10 times, each extraction time is 1-2h;
[0068] (2) Filter the extract obtained in step (1) with a filter bag of 300-400 mesh, and pass the filtrate through the series connection o...
Embodiment 3
[0078] A method for synchronously preparing four effective parts of the Anemarrhena Phellodendron herb pair. The four effective parts are respectively total polysaccharide extract, total saponin extract, total flavonoid extract, and total alkaloid extract. The simultaneous preparation method includes Follow the steps below:
[0079] (1) Crush Anemarrhena anemarrhena and Cortex Phellodendri (5kg and 6kg respectively) with a weight ratio of 1:1.2 to 10-120 mesh, soak in ethanol with a volume concentration of 80% for 2-3 hours, and reflux (control the temperature at 80- 100°C) for 4 extractions, then reflux with 30% ethanol (temperature controlled at 80-100°C) for 5 extractions, and combine the extracts; the amount of ethanol used for each extraction is the total weight of Anemarrhena and Phellodendri 6-10 times, each extraction time is 1-2h;
[0080] (2) Filter the extract obtained in step (1) with a filter bag of 300-400 mesh, and pass the filtrate through the series connectio...
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