Evaporation furnace capable of shortening distance and rapidly increasing and reducing temperature, and manufacturing method thereof

A heating and cooling, short-distance technology, applied in the field of adjustable short-distance rapid heating and cooling evaporation furnace and its manufacturing, can solve the problem of inability to solve the phenomenon of solid phase sublimation and the like

Inactive Publication Date: 2013-08-28
合肥科晶材料技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] At present, in a series of material research fields such as photovoltaics and semiconductors, coatings run through the entire material research industry, and vapor deposition is the most extensive research direction. At present, the research field has new directions, and more material research directions are concentrated on solid-state materials. and liquid deposition sources, and the current vapor deposition equipment, due to the high desublimation temperature and fast desublimation speed after the solid material is vaporized, in the previous vapor deposition equipment, it is impossible to solve the problem of high temperature gas phase solid during the transmission process. Phase desublimation phenomenon and the large gradient temperature field required for solid phase deposition in a short distance and the problem of achieving control of deposition thickness and film uniformity

Method used

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  • Evaporation furnace capable of shortening distance and rapidly increasing and reducing temperature, and manufacturing method thereof
  • Evaporation furnace capable of shortening distance and rapidly increasing and reducing temperature, and manufacturing method thereof
  • Evaporation furnace capable of shortening distance and rapidly increasing and reducing temperature, and manufacturing method thereof

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] see figure 1 and figure 2 , an adjustable short-distance rapid heating and cooling evaporation furnace provided by the present invention includes a trough-shaped support 1, a lower heating table bottom plate 2 is installed in the bottom inner cavity of the trough-shaped support 1, and the upper part of the lower heating table bottom plate 2 is installed There is a lower heating table 3, and the lower part is equipped with a rotary drive device 4 that can drive the lower heating table 3 to rotate horizontally. Guide rails 5 are arranged on both sides of the grooved support 1, and an upper heating table that can move up and down along it is installed between the guide rails 5. A platform base plate 6, the bottom of the upper heating platform base plate 6 is provided with an upper heating platform 7 opposite to the lower heating platform 3, and the upper part is equipped with a mobile driving device 8 that can drive the upper heating platform 7 to move up and down;

[00...

Embodiment 2

[0026] The difference between this embodiment and Embodiment 1 is that the sample loading stage 7i includes an internal quartz / graphite / oxide, nitride ceramic stage 7i-1, and the internal quartz / graphite / oxide, nitride The ceramic stage 7i-1 is detachably installed in the stainless steel sample stage 7i-2, and the stainless steel sample stage 7i-2 is mounted on the bottom of the upper heating stage 7 by using locking bolts.

Embodiment 3

[0028] The difference between this embodiment and Embodiment 1 is that a series of heating elements such as SiC, MoSi2, Mo, Ta or W can also be installed in the lower heating platform 3 and the upper heating platform 7 to improve the heating effect. (Short-wave infrared lamps can reach 1100°C as heating elements, SiC, MoSi 2 , Mo, Ta and W heating elements can reach a maximum temperature of 1900°C. )

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Abstract

The invention discloses an evaporation furnace capable of shortening distance and rapidly increasing and reducing temperature, and a manufacturing method thereof. The evaporation furnace comprises an upper heating table and a lower heating table, wherein the upper heating table and the lower heating table are oppositely arranged inside a slot groove up and down; the heating table has the freedom of moving up and down along the slot bracket; the lower heating table has the freedom of rotating along the bottom part of the slot bracket; a sample table capable of loading an evaporation substrate is arranged at the bottom part of the upper heating table; an evaporation source opposite to the sample table is arranged at the top part of the lower heating table; short-wave infrared lamp tubes are inserted into the upper heating table and the lower heating table; and an air inlet and outlet and a cooling water inlet and outlet communicated with the heating tables are arranged inside the upper heating table and the lower heating table. The upper and lower heating tables can achieve the temperature difference which is much greater than that of the traditional equipment within the shortest distance by utilizing up and down opposite mode of dual temperature fields and using a water-cooling cavity; and the evaporation distance and the temperature difference of the upper and lower temperature fields are increased and reduced by adjusting the distance between the upper and lower heating tables, so that adjustable solid-phase evaporation is achieved.

Description

technical field [0001] The invention relates to an evaporation furnace and a manufacturing method thereof, in particular to an adjustable short-distance rapid heating and cooling evaporation furnace and a manufacturing method thereof. Background technique [0002] At present, in a series of material research fields such as photovoltaics and semiconductors, coatings run through the entire material research industry, and vapor deposition is the most extensive research direction. At present, the research field has new directions, and more material research directions are concentrated on solid-state materials. and liquid deposition sources, and the current vapor deposition equipment, due to the high desublimation temperature and fast desublimation speed after the solid material is vaporized, in the previous vapor deposition equipment, it is impossible to solve the problem of high temperature gas phase solid during the transmission process. The phase desublimation phenomenon and ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C14/28
Inventor 邾根祥江晓平王伟
Owner 合肥科晶材料技术有限公司
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