A method for low-temperature modification of c/c composite materials by ultrasonic-ultraviolet method
A technology of composite materials and carbon composite materials, which is applied in the field of low-temperature modification of C/C composite materials by ultrasonic-ultraviolet method, can solve the problems of C/C composite materials such as degradation of mechanical and thermal properties, protection failure, and volatile compounds. Achieve the effect of low raw material price, improved anti-oxidation performance, and improved anti-oxidation performance
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Embodiment 1
[0021] 1) Take the 2D-carbon / carbon composite material used in aircraft brake pads and process it into 10×10×3mm 3 The small cubes were polished and chamfered on the surface, then cleaned with absolute ethanol and deionized water in an ultrasonic generator, and dried in an oven for later use;
[0022] 2) Mix the analytically pure tri-n-butyl borate and absolute ethanol at a volume ratio of 1:6, and keep stirring, record as A;
[0023] 3) Mix A with analytically pure acetic acid at a volume ratio of 2.5:1 and keep stirring to form a sol precursor, which is denoted as B;
[0024] 4) Add 10% ZrB of B mass to B 2 Powder, stir for 1-2 hours to form a uniform suspension C;
[0025] 5) Pour the suspension C into a four-neck round bottom flask, and place the 2D-carbon / carbon composite material in the suspension C, and put the equipped four-neck round bottom flask into a UWave-1000 microwave·ultraviolet· The ultrasonic trinity synthesis extraction reaction instrument is fixed, and t...
Embodiment 2
[0028] 1) Take the 2D-carbon / carbon composite material used in aircraft brake pads and process it into 10×10×3mm 3 The small cubes were polished and chamfered on the surface, then cleaned with absolute ethanol and deionized water in an ultrasonic generator, and dried in an oven for later use;
[0029] 2) Mix the analytically pure tri-n-butyl borate and absolute ethanol at a volume ratio of 1:4, and keep stirring, record as A;
[0030] 3) Mix A with analytically pure acetic acid at a volume ratio of 2:1, and keep stirring to form a sol precursor, which is denoted as B;
[0031] 4) Add 10% ZrB of B mass to B 2 Powder, stir for 1-2 hours to form a uniform suspension C;
[0032] 5) Pour the suspension C into a four-neck round bottom flask, and place the 2D-carbon / carbon composite material in the suspension C, and put the equipped four-neck round bottom flask into a UWave-1000 microwave·ultraviolet· The ultrasonic trinity synthesis extraction reaction instrument is fixed, and th...
Embodiment 3
[0035] 1) Take the 2D-carbon / carbon composite material used in aircraft brake pads and process it into 10×10×3mm 3 The small cubes were polished and chamfered on the surface, then cleaned with absolute ethanol and deionized water in an ultrasonic generator, and dried in an oven for later use;
[0036] 2) Mix the analytically pure tri-n-butyl borate and absolute ethanol at a volume ratio of 1:3, and keep stirring, record as A;
[0037]3) Mix A with analytically pure acetic acid at a volume ratio of 4:1 and keep stirring to form a sol precursor, which is denoted as B;
[0038] 4) Add 10% ZrB of B mass to B 2 Powder, stir for 1-2 hours to form a uniform suspension C;
[0039] 5) Pour the suspension C into a four-neck round bottom flask, and place the 2D-carbon / carbon composite material in the suspension C, and put the equipped four-neck round bottom flask into a UWave-1000 microwave·ultraviolet· The ultrasonic trinity synthesis extraction reaction instrument is fixed, and the ...
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