Method and device for preparing solar-grade polysilicon by electron beam continuous melting
An electron beam melting and electron beam melting furnace technology is applied in the field of electron beam continuous melting to prepare solar-grade polysilicon, which can solve the problems of energy loss, lowering production efficiency, etc. Effect
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Embodiment 1
[0022] Such as figure 1 As shown, the device for preparing solar-grade polysilicon by electron beam continuous smelting includes a furnace body 1. A water-cooled melting crucible 2 is arranged on the inner upper part of the furnace body 1. One side of the melting crucible 2 has a concave melting pool. The other side of the melting crucible 2 is a downwardly inclined diversion area; the top of the furnace body 1 above the melting crucible 2 is connected with an electron gun 3 for melting and an electron gun 4 for melting, and the furnace located on the side of the melting pool of the melting crucible 2 The side wall of the body 1 is connected with a feeding mechanism 5, and the outlet of the feeding mechanism 5 is located above the melting pool; the bottom of the furnace body 1 below the pouring port of the diversion area is provided with a solidification crucible 6.
[0023] Wherein, the melting crucible 2 is a copper crucible with water cooling. The use of the copper crucibl...
Embodiment 2
[0027] Adopt the device described in embodiment 1, carry out electron beam continuous smelting and prepare solar grade polysilicon, carry out according to the following steps:
[0028] (1) Material preparation: Clean 500kg of silicon material with a phosphorus content of 0.005% using cleaning equipment to remove dust and oil stains on the surface, put it into a drying box, and dry it at 80°C. Put the dried silicon material into the material box of the feeding mechanism 5 and the melting crucible 2 respectively, wherein, put 5 kg in the melting crucible 2 as the melting base material, and put 10 kg in the solidification crucible 6 that has been melted by electron beams The purified silicon material is used as the solidified bottom material;
[0029] (2) Pretreatment: Combine the device with the furnace, start the cooling water circulation for the electron beam melting furnace, the melting crucible 2 and the solidification crucible 6, and start the vacuum system of the electron ...
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