LAMP detection reagent for transgenosis carica papaya GMYK strain
A technology for detecting reagents and papaya, which is applied in the field of reagents for detecting papaya, and achieves the effects of intuitive results, simple operation, and low determination difficulty.
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Embodiment 1
[0015] Embodiment 1, the LAMP detection reagent of transgenic papaya GM YK strain
[0016] 25 μL reaction system: 2.5 μL of 10×LAMP reaction buffer, 1.5 μL of Bst DNA polymerase at a concentration of 8 U / L, 4.0 μL of dNTP at a concentration of 2.5 mmol / L, and MgCl at a concentration of 25 mmol / L 2 2.5 μL, 4.0 μL of betaine with a concentration of 5.0 mol / L, 0.2 μL each of FIP and BIP with a concentration of 20 μmol / L, 1.6 μL each of F3 and B3 with a concentration of 20 μmol / L, both with a concentration of 20 μmol / L 0.8 μL each for Loop1 and Loop2. LAMP reaction buffer and Bst DNA polymerase were purchased from NEW ENGLAND Biolabs, dNTP Bao Bioengineering (Dalian) Co., Ltd., and betaine was purchased from Shanghai Sinopharm Chemical Reagent Co., Ltd.
Embodiment 2
[0017] Embodiment 2, DNA extraction
[0018] Papaya DNA was extracted according to the operating instructions of the Dneasy Plant Mini Kit reagent (purchased from QIAGEN, Germany): (1) Weigh 200 mg of the sample, homogenize the sample by bead milling, and put it into a 1.5 mL centrifuge tube; (2) Add 500 μL of buffer AP1, and shake in a 65°C oscillating constant temperature metal bath for 15 minutes; (3) Add 130 μL of buffer AP2, mix thoroughly by inverting up and down, and let stand in a refrigerator at 4°C for 5 minutes; (4) Use 12 000 Centrifuge at room temperature for 5 min at r / min, transfer 500 μL of the supernatant to a 2 mL collection tube; (5) Put the collection tube into the QIAcube automatic nucleic acid extraction instrument, select the DNeasy Plant Mini mode, and automatically extract DNA using U-0080D Determination of OD by biospectrophotometer 260 and OD 280 Calculate the DNA concentration; (6) Take out the DNA sample template and store it in a -20°C refrigera...
Embodiment 3
[0019] Embodiment 3, LAMP detection
[0020] We bought papayas or processed products from Ningbo Supermarket: Hainan papaya, red heart papaya, Dole papaya, Thai papaya, Guangxi green papaya, Risheng papaya, Tainong papaya, Leqi dried papaya, Taiwan green papaya powder, etc. The LAMP detection of the present invention is used for detection. The detection method includes DNA extraction as in Example 2. Take 2 μL of each DNA template, and use the detection reagent of Example 1 to perform LAMP detection respectively. The amplification cycle parameters are: preheating at 50°C for 1 min ;React at 61°C for 1.5 min, run for 40 cycles, use the accumulation of fluorescent signals to monitor the LAMP reaction process in real time, drop 0.1 μL of staining agent SYBR Green I (10 000×) on the cap of the reaction tube, SYBR Green I must not contact with the mixture. After the amplification, centrifuge at 8 000 r / min for 1 min to fully mix the dye with the amplification product, and observe ...
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