Adhesive layer for optical film and method for producing same, adhesive optical film and method for producing same, image display device, and coating liquid supply device
An optical film and adhesive layer technology, applied in film/sheet adhesive, pressure-sensitive film/sheet, optics, etc., can solve the problems of a lot of time and labor, insufficient bubble removal, etc. The effect of high efficiency, prolonging life and improving removal efficiency
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Embodiment 1)
[0130] In Example 1, a water-dispersed acrylic adhesive was used as the adhesive coating liquid. When preparing the water-dispersed acrylic adhesive, 55554 parts of butyl acrylate, 2776 parts of acrylic acid, 1665 parts of mono[poly(propyleneoxy) methacrylate] phosphate ( The average degree of polymerization of the propyleneoxy group is 5.0), and 5 parts of 3-methacryloxypropyl-triethoxysilane, etc. (manufactured by Shin-Etsu Chemical Co., Ltd., KBM-503) and mixed to obtain a single body mixture. Next, 1,300 parts of AQUARON HS-10 (manufactured by Daiichi Kogyo Pharmaceutical Co., Ltd.) and 38,700 parts of ion-exchanged water were added as a reactive emulsifier to 60,000 parts of the prepared monomer mixture. Co., Ltd.), and stirred at 7000 rpm for 10 minutes to prepare a monomer emulsion. Then, in the reaction container equipped with a condenser tube, a nitrogen gas introduction tube, a thermometer, a dropping funnel, and a stirring blade, 20,000 parts and 35,000 parts of i...
Embodiment 2~9)
[0137] In the same manner as in Example 1, except that the filtration accuracy, the presence or absence of a gradient of filtration accuracy, and the pressure difference were changed to those in Table 1, the above-mentioned adhesive containing a water-dispersed acrylic adhesive The coating liquid is filtered (filtering step).
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