Special grease composition for dual mass flywheel and preparation method thereof
A dual-mass flywheel and grease technology, which is applied in the field of grease, can solve problems such as no grease products, and achieve excellent lubrication, excellent anti-rust performance, and good high-temperature oxidation resistance.
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Embodiment 1
[0023]
[0024]
[0025] 400 grams of 12-hydroxystearic acid, 100 grams of azelaic acid and 700 grams of PAO (40°C viscosity 400mm 2 / s) into the reactor, heated to 90-100°C, and 102 grams of lithium hydroxide was dissolved in five times of water to prepare an alkaline solution. Add lye at 90°C of the reaction kettle, close all valves of the reaction kettle, increase the temperature and pressure, increase the pressure to 0.5-0.6MPa, heat up to 120-130°C and start constant temperature and constant pressure for 160-180 minutes. After the constant temperature is over, the temperature is increased and the pressure is released, and the pressure is released to normal pressure. At 130 to 140 ° C, 25 grams of polyisobutylene and 12.5 grams of titanium dioxide are added, and the temperature is kept constant for one hour to achieve the purpose of composite co-crystallization. After the constant temperature is over, continue to heat up, the material is heated to 200-210 °C, and the...
Embodiment 2
[0030]
[0031]
[0032] Mix 400 grams of 12-hydroxystearic acid, 100 grams of sebacic acid and 800 grams of PAO (40°C viscosity 400mm 2 / s) into the reaction kettle, heated to 90-100 °C, and 98 grams of lithium hydroxide was dissolved in five times of water to prepare an alkaline solution. Add lye at 90°C of the reaction kettle, close all valves of the reaction kettle, increase the temperature and pressure, increase the pressure to 0.5-0.6MPa, heat up to 120-130°C and start constant temperature and constant pressure for 160-180 minutes. After the constant temperature is over, the temperature is increased and the pressure is released, and the pressure is released to normal pressure. At 130-140 °C, 28 grams of polyisobutylene and 14 grams of titanium dioxide are added, and the temperature is kept constant for one hour to achieve the purpose of composite co-crystallization. After the constant temperature is over, continue to heat up, the material is heated to 200-210 °C, a...
Embodiment 3
[0037]
[0038]
[0039] Mix 400 g of 12-hydroxystearic acid, 100 g of azelaic acid and 750 g of ester oil (viscosity 380mm at 40°C) 2 / s) into the reactor, heated to 90-100°C, and 102 grams of lithium hydroxide was dissolved in five times of water to prepare an alkaline solution. Add lye at 90°C of the reaction kettle, close all valves of the reaction kettle, increase the temperature and pressure, increase the pressure to 0.5-0.6MPa, heat up to 120-130°C and start constant temperature and constant pressure for 160-180 minutes. After the constant temperature is over, the temperature is increased and the pressure is released, and the pressure is released to normal pressure. At 130-140 °C, 27 grams of polyisobutylene and 13.5 grams of titanium dioxide are added, and the temperature is kept constant for one hour to achieve the purpose of composite co-crystallization. After the constant temperature is over, continue to heat up, the material is heated to 200-210 ° C, and then...
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