Method for improving corrosion resistance of neodymium-iron-boron magnetic body

A technology of neodymium iron boron and magnets, which is applied to the surface coating liquid device, metal material coating process, pretreatment surface, etc., can solve the problems of coating treatment, light weight, and inability to improve anti-corrosion performance Effect

Active Publication Date: 2014-01-08
NINGBO YUNSHENG BONDED MAGNET CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, NdFeB magnets with a single weight of no more than 0.1 grams (hereinafter referred to as NdFeB magnets) are too light to be coated. Most of the surface anticorrosion of NdFeB small magnets adopts traditional pretreatment processes and The combination of rolling and spraying process, the specific process is: degreasing (remove the grease on the surface of the magnet) → ultrasonic washing (clean the degreasing liquid on the surface of the magnet) → rust removal (remove the rust on the surface of the magnet) → ultrasonic washing (remove the grease on the surface of the magnet) Descaling solution) → surface adjustment (adjust the metal activity on the surface of the magnet to the maximum) → phosphating at room temperature (forming a phosphating film on the surface of the magnet) → washing with pure water at room temperature (removing the phosphating s

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Embodiment 1: A tile-shaped NdFeB magnet with a size of outer R1.85mm × inner R1.95mm × width 2.8mm × length 3.8mm is selected, and the unit weight of the NdFeB magnet is 0.029 grams. The surface of NdFeB magnets is treated with anti-corrosion to improve its anti-corrosion performance.

[0024] A method for improving the anticorrosion performance of an NdFeB magnet, comprising the following steps:

[0025] ① Degreasing: Degrease the NdFeB magnet to be treated, and the pH value of the degreasing solution is 9;

[0026] ②The first ultrasonic washing: perform the first ultrasonic washing on the degreased NdFeB magnet;

[0027] ③ Derusting: Derusting the NdFeB magnets after the first ultrasonic washing, the PH value of the derusting solution is 2;

[0028] ④Second ultrasonic washing: perform the second ultrasonic washing on the derusted NdFeB magnet;

[0029] ⑤Surface adjustment: The NdFeB magnet after the second ultrasonic washing is subjected to surface adjustment trea...

Embodiment 2

[0038] Embodiment 2: A tile-shaped NdFeB magnet with a size of outer R1.85mm × inner R1.95mm × width 2.8mm × length 3.8mm is selected, and the single weight of the NdFeB magnet is 0.029 grams. The surface of NdFeB magnets is treated with anti-corrosion to improve its anti-corrosion performance.

[0039] A method for improving the anticorrosion performance of an NdFeB magnet, comprising the following steps:

[0040] ① Degreasing: Degrease the NdFeB magnet to be treated, and the pH value of the degreasing solution is 11;

[0041] ②The first ultrasonic washing: perform the first ultrasonic washing on the degreased NdFeB magnet;

[0042] ③ Rust removal: The NdFeB magnet after the first ultrasonic washing is subjected to rust removal treatment, and the PH value of the rust removal solution is 4;

[0043] ④Second ultrasonic washing: perform the second ultrasonic washing on the derusted NdFeB magnet;

[0044] ⑤Surface adjustment: The NdFeB magnet after the second ultrasonic washin...

Embodiment 3

[0053] Embodiment 3: Select the tile-shaped NdFeB magnet whose size is outer R1.85mm × inner R1.95mm × width 2.8mm × length 3.8mm, the unit weight of the NdFeB magnet is 0.029 grams, and the following method is used to The surface of NdFeB magnets is treated with anti-corrosion to improve its anti-corrosion performance.

[0054] A method for improving the anticorrosion performance of an NdFeB magnet, comprising the following steps:

[0055] ① Degreasing: Degrease the NdFeB magnet to be treated, and the pH value of the degreasing solution is 11;

[0056] ②The first ultrasonic washing: perform the first ultrasonic washing on the degreased NdFeB magnet;

[0057] ③ Rust removal: The NdFeB magnet after the first ultrasonic washing is subjected to rust removal treatment, and the PH value of the rust removal solution is 3;

[0058] ④Second ultrasonic washing: perform the second ultrasonic washing on the derusted NdFeB magnet;

[0059] ⑤Surface adjustment: The NdFeB magnet after th...

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Abstract

The invention discloses a method for improving corrosion resistance of a neodymium-iron-boron magnetic body. The method comprises the following steps: degreasing; performing first ultrasonic water washing; derusting; performing second ultrasonic water washing; performing surface conditioning; performing medium and high temperature phosphating, wherein the pH value of a phosphating solution is 2-4, the concentration of the phosphating solution is 8-20%, the temperature is 60-80 DEG C, and the phosphating time is 10-30min; performing medium and high temperature pure water washing, wherein the temperature of medium and high temperature pure water is 60-90 DEG C, the water washing time is 30-120s, and the electric conduction of the medium and high temperature pure water is not more than 50us/cm; passivating; performing normal temperature pure water washing; drying; soaking in an anti-rust agent, wherein the neodymium-iron-boron magnetic body after drying at normal temperature is soaked in the anti-rust agent with the concentration of 100%, and the soaking time is 10-40min; and carrying out blow drying or drying. The method has the advantages that the anti-rust agent is permeated into a phosphating layer, and a dense corrosion-resistant layer with an anti-oxidation function is formed on the neodymium-iron-boron magnetic body; compared with a traditional way of combining a pretreatment process with a roll-spraying process in the prior art, the corrosion resistance of the product is greatly improved.

Description

technical field [0001] The invention relates to a method for improving anticorrosion performance, in particular to a method for improving anticorrosion performance of NdFeB magnets. Background technique [0002] NdFeB magnets have excellent magnetic properties and high cost performance, and are widely used in technical fields such as electronics, motors and communications. However, the nature of NdFeB magnets is very lively, and the density of NdFeB magnetic powder is much lower than that of steel, the porosity is very high, the pore size is relatively large, and it is easy to be corroded, which will cause problems such as rust, powdering or loss of magnetism. , which greatly limits the service life and application fields of NdFeB magnets. [0003] At present, in order to improve the anti-corrosion performance of NdFeB magnets, the surface is generally coated (including electroplating, electrophoresis and spraying, etc.). However, NdFeB magnets with a single weight of no m...

Claims

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Application Information

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IPC IPC(8): C23C22/73C23C22/83B05D3/10
Inventor 邓颖华赵春伟王江
Owner NINGBO YUNSHENG BONDED MAGNET CO LTD
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