Method for synthesizing NaA zeolite membrane with high membrane forming efficiency
A zeolite membrane and membrane-forming technology, applied in chemical instruments and methods, membrane technology, semi-permeable membrane separation, etc., can solve the problems of reducing the separation performance of synthetic membranes, unable to completely eliminate pore defects on the carrier surface, and achieve high membrane-forming rate Effect
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[0036] Example 1
[0037] A method for preparing NaA zeolite membrane by vacuum filtration of seed crystals. The preparation steps are as follows:
[0038] 1. Take α-Al 2 O 3 The outer surface of the carrier tube is smoothed with 1200# sandpaper successively, and then the polished α-Al 2 O 3 The carrier tube was immersed in 0.1 mol / L hydrochloric acid solution and 0.1 mol / L sodium hydroxide solution successively, and ultrasonically vibrated for 0.5 hours respectively. After taking it out, it was washed with deionized water until it became neutral, and it was dried in an oven at 50°C for 16 hours. Calcined in a Furnace at 200°C for 2h, and take it out for later use.
[0039] 2. Use NaA molecular sieve seed crystals and deionized water to prepare a 0.1g / L seed crystal aqueous solution, and use ultrasonic dispersion for the obtained solution for 2 hours, and then stand for 12 hours. stand-by.
[0040] 3. Seal both ends of the carrier tube with polytetrafluoroethylene. Heat it at 150°C...
Example Embodiment
[0044] Example 2
[0045] A method for preparing NaA zeolite membrane by vacuum filtration of seed crystals. The preparation steps are as follows:
[0046] 1. Take α-Al 2 O 3 The outer surface of the carrier tube is smoothed with 1200# sandpaper successively, and then the polished α-Al 2 O 3 The carrier tube was immersed in 0.8 mol / L hydrochloric acid solution and 0.8 mol / L sodium hydroxide solution successively, ultrasonically vibrated for 1 hour respectively, and washed with deionized water to neutrality after being taken out, and dried in an oven at 80°C for 20 hours. The furnace was calcined at 280°C for 3h, and then taken out for use.
[0047] 2. Use NaA molecular sieve seed crystals and deionized water to prepare a 0.5g / L seed crystal aqueous solution, and use ultrasonic dispersion for the obtained solution for 4 hours, and then stand for 18 hours. stand-by.
[0048] 3. Seal both ends of the carrier tube with polytetrafluoroethylene. Heat it at 170°C for 3h, take it out and q...
Example Embodiment
[0052] Embodiment 3
[0053] A method for preparing NaA zeolite membrane by vacuum filtration of seed crystals. The preparation steps are as follows:
[0054] 1. Take α-Al 2 O 3 The outer surface of the carrier tube is smoothed with 1200# sandpaper successively, and then the polished α-Al 2 O 3 The carrier tube was immersed in 0.8mol / L hydrochloric acid solution and 0.8mol / L sodium hydroxide solution successively, ultrasonically vibrated for 1h respectively, and then washed with deionized water to neutrality after being taken out, dried in an oven at 90℃ for 24h, and then in the muffle The furnace was calcined at 350°C for 4h, and then taken out for use.
[0055] 2. Use NaA molecular sieve seed crystals and deionized water to prepare 0.8 g / L seed crystal aqueous solution, and the obtained solution is dispersed by ultrasonic for 5 hours, and then left to stand for 20 hours. stand-by.
[0056] 3. Seal both ends of the carrier tube with polytetrafluoroethylene. Heat it at 200°C for 3h...
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