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Concrete chemical-selfreparing microcapsule and preparation method thereof

A self-repairing microcapsule and concrete technology, applied in the field of concrete corrosion inhibitor capsules, can solve the problem of corrosion inhibitor loss effect, etc., and achieve the effect of slow release effect, green environmental protection, delaying concrete carbonization and steel corrosion inhibition, and good stability.

Active Publication Date: 2014-02-26
SHENZHEN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] Some scholars proposed to add corrosion inhibitors during the preparation of reinforced concrete, among which nitrite is a typical representative, but using this method, the large loss of corrosion inhibitors in the early stage makes its effect on steel corrosion inhibition very small

Method used

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  • Concrete chemical-selfreparing microcapsule and preparation method thereof
  • Concrete chemical-selfreparing microcapsule and preparation method thereof
  • Concrete chemical-selfreparing microcapsule and preparation method thereof

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preparation example Construction

[0035] One, the embodiment of the preparation method of concrete chemical self-healing microcapsules:

[0036] 1. Preparation of capsule core:

[0037] Table 1. The mass ratio of raw materials in each embodiment of the capsule core

[0038]

[0039]

[0040] in:

[0041] Calcium hydroxide (Chengdu Kelong Chemical Reagent Factory, analytically pure);

[0042] Ethanol (Chengdu Kelong Chemical Reagent Factory, analytically pure) was used as a solvent;

[0043] Microcrystalline cellulose (Anhui Shanhe Pharmaceutical Excipients Co., Ltd., Shanhe brand) was used as a thickener;

[0044] Tween 80 (Guangdong Yueqiao Reagent Plastic Co., Ltd., Yueqiao brand) was used as a dispersant;

[0045] Hydroxypropyl methylcellulose (Shandong Ningjin Dexin Cellulose Co., Ltd.) was used as a binder.

[0046] The capsule core preparation method comprises the following steps:

[0047] 1) Capsule core preparation: according to the capsule core mix ratio in Table 1, first fully mix 50% eth...

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Abstract

The invention discloses a concrete chemical-selfreparing microcapsule and a preparation method thereof. The concrete chemical-selfreparing microcapsule comprises a capsule core and a coating, the capsule core comprises a water soluble alkali and a forming agent, the coating comprises an organic material sensitive to low alkali environment, the water soluble alkali is one or a plurality of substances from calcium hydroxide, sodium hydroxide and potassium hydroxide. The concrete chemical-selfreparing microcapsule has good stability, by changing of the mass ratio of the capsule core material and the coating material, the release rate of the corrosion inhibitor can be controllably optimized, the water soluble alkali is used for enhancing PH to achieve the purposes of steel bar corrosion inhibition and delaying of the concrete carbonation, and the used materials are green and environmentally friendly, so that the concrete chemical-selfreparing microcapsule has the effects of controllable optimization, long effective period, good sustained-release effect and green and environmental protection effect.

Description

[technical field] [0001] The invention relates to a concrete corrosion inhibitor capsule, in particular to a concrete chemical self-repairing microcapsule and a preparation method thereof. [Background technique] [0002] As a representative of traditional building materials, reinforced concrete has the characteristics of high compressive strength, high durability, and low cost. It is widely used in industrial and civil buildings, bridges, road engineering, underground engineering, water conservancy and hydropower engineering, ports and marine engineering, etc. Structures are now infiltrating into long-span structures, towering structures, giant structures and special structures, and are the most widely used building materials. In the in-service concrete structure, with long-term use and the influence of the surrounding complex environment, especially in the coastal environment, the steel bars embedded in the concrete will inevitably corrode, resulting in a significant reduct...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B24/38C04B24/28C04B22/06
Inventor 董必钦邢锋丁蔚健李淑婷吴永潮王琰帅房国豪简震昭林立
Owner SHENZHEN UNIV
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