Composition having high refraction
A composition and high refraction technology, applied in the direction of instruments, electrical components, circuits, etc., can solve the problems of inability to maintain stable dispersion of metal oxide particles, particle sinking, heat resistance, weather resistance decline, etc.
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Embodiment 1
[0114] A silicone resin was prepared by sol-gel polymerizing 300 mmol of methyltrimethoxysilane and 300 mmol of tetramethoxysilane in the presence of an acid catalyst. Then, 2 g of the prepared resin and 8 g of poly(dibutyltitanate) (polymerization degree: n=4) were dissolved in 10 g of ethylene glycol diethyl ether to prepare a curable composition. Then, the composition was spin-coated and cured at a temperature of 200° C. for 30 minutes, thereby forming a high-refractive film.
Embodiment 2
[0116] In addition to using 8g of di-n-butoxide ethyl acetate (titanium di-n-butoxide (bis-2,4-pentanedionate)) instead of poly (butyl titanate), in the same manner as in Example 1 A high refractive film was prepared in the same manner as described.
Embodiment 3
[0118] A high refractive film was prepared in the same manner as described in Example 1 except that 8 g of zirconium tert-butoxide was used instead of poly(butyl titanate).
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