A slow-release polycarboxylate water reducer, its preparation method and use method
A slow-release polycarboxylic acid and water-reducing agent technology, which is applied in the field of building materials, can solve problems such as unsatisfactory slow-release effects, and achieve the effects of large-scale industrial production, good fluidity retention, and simple process
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Embodiment 1
[0038] (1) Preparation before polymerization:
[0039] Preparation of solution A: Weigh 6 parts by weight of acrylic acid, 1.80 parts by weight of methacrylic acid, 9.50 parts by weight of hydroxyethyl acrylate, 5.40 parts by weight of hydroxypropyl acrylate and 39 parts by weight of water, stir and mix evenly, and prepare dropwise;
[0040] Preparation of solution B: Weigh 0.30 parts by weight of L-ascorbic acid, 0.85 parts by weight of mercaptoacetic acid, 0.15 parts by weight of mercaptopropionic acid and 71 parts by weight of water, stir and mix evenly, and prepare dropwise;
[0041] Preparation of mixture C: Weigh 100 parts of unsaturated polyether DD-417 with a number average molecular weight of 1200, 1.00 parts of hydrogen peroxide (concentration: 30wt%) and 75 parts of water, put them into a polymerization reactor, stir evenly, and prepare for polymerization;
[0042] (2) Polymerization: Introduce protective gas nitrogen into the polymerization reactor that has been pu...
Embodiment 2~ Embodiment 5
[0046] According to the method and steps of Example 1, the slow-release polycarboxylate water-reducer of the present invention was prepared according to the formula in Table 1, and the obtained polycarboxylate water-reducer was added according to the amount shown in Table 1. In the cement paste and concrete, the performance data of the obtained cement paste and concrete are also shown in Table 1.
[0047] Table 1 (the dosage units of each component are parts by weight)
[0048]
[0049]
[0050] It can be seen from Table 1 that the slow-release polycarboxylate superplasticizer of the present invention has good slow-release properties, fluidity retention and slump retention.
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