Fabric formaldehyde-free fixing agent and preparation method thereof

A formaldehyde-free color-fixing agent and fabric technology, which can be used in dyeing, textiles, and papermaking. It can solve the problems of fabric staining, easy fading, and old fabrics, and achieve the effect of improving washing fastness and simple preparation process.

Active Publication Date: 2014-03-26
JIANGSU ZHONGXIN RESOURCES GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the process of fabric weaving, although some dyes are brighter in color, due to the poor fastness of wet treatment, the phenomenon of fading and sticking is more serious, which not only makes the fabric itself look old, but also easily fades when it meets water. Easy to cause staining with other fabrics

Method used

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  • Fabric formaldehyde-free fixing agent and preparation method thereof

Examples

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Embodiment 1

[0014] A fabric formaldehyde-free color-fixing agent, comprising the following components in parts by weight: 15 parts of n-butyl acrylate, 5 parts of chitosan quaternary ammonium salt, 6 parts of isobornyl methacrylate, acryloyloxyethyl 7 parts of trimethylammonium chloride, 8 parts of triallylamine, 2 parts of vinyl siloxane, 3 parts of glacial acetic acid, 0.1 part of azobisisobutylcyanide, and 100 parts of deionized water.

[0015] The preparation method of the present embodiment fabric formaldehyde-free color-fixing agent comprises the steps:

[0016] (1) Dissolve acryloyloxyethyltrimethylammonium chloride and triallylamine in some deionized water, then add azobisisobutylcyanide, and react at 40°C for 1 hour to obtain a reaction solution;

[0017] (2) Continue to add n-butyl acrylate, chitosan quaternary ammonium salt, isobornyl methacrylate, vinyl siloxane and the remaining deionized water to the reaction solution obtained in step (1), keeping the temperature at At 60°C...

Embodiment 2

[0019] A fabric formaldehyde-free color-fixing agent, comprising the following components in parts by weight: 25 parts of n-butyl acrylate, 9 parts of chitosan quaternary ammonium salt, 10 parts of isobornyl methacrylate, acryloyloxyethyl 14 parts of trimethylammonium chloride, 10 parts of triallylamine, 5 parts of vinyl siloxane, 5 parts of glacial acetic acid, 1 part of azobisisobutylcyanide, and 120 parts of deionized water.

[0020] The preparation method of the present embodiment fabric formaldehyde-free color-fixing agent comprises the steps:

[0021] (1) Dissolve acryloyloxyethyltrimethylammonium chloride and triallylamine in some deionized water, then add azobisisobutylcyanide, and react at 60°C for 2 hours to obtain a reaction solution;

[0022] (2) Continue to add n-butyl acrylate, chitosan quaternary ammonium salt, isobornyl methacrylate, vinyl siloxane and the remaining deionized water to the reaction solution obtained in step (1), keeping the temperature at Keep ...

Embodiment 3

[0024] A fabric formaldehyde-free color-fixing agent, comprising the following components in parts by weight: 20 parts of n-butyl acrylate, 7 parts of chitosan quaternary ammonium salt, 8 parts of isobornyl methacrylate, acryloyloxyethyl 12 parts of trimethylammonium chloride, 9 parts of triallylamine, 4 parts of vinyl siloxane, 4 parts of glacial acetic acid, 0.5 parts of azobisisobutylcyanide, and 110 parts of deionized water.

[0025] The preparation method of the present embodiment fabric formaldehyde-free color-fixing agent comprises the steps:

[0026] (1) Dissolve acryloyloxyethyltrimethylammonium chloride and triallylamine in some deionized water, then add azobisisobutylcyanide, and react at 50°C for 1.5h to obtain a reaction solution;

[0027] (2) Continue to add n-butyl acrylate, chitosan quaternary ammonium salt, isobornyl methacrylate, vinyl siloxane and the remaining deionized water to the reaction solution obtained in step (1), keeping the temperature at At 45°C...

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Abstract

The invention relates to a fabric formaldehyde-free fixing agent, and a preparation method thereof, and belongs to the technical field of textile auxiliary agents. The fixing agent comprises the following components in parts by weight: 15-25 parts of crylic acid butyl ester, 5-9 parts of chitosan hyamine, 6-10 parts of isobornyl acrylate, 7-14 parts of acrylyl oxyethyl acrylate trimethyl ammonium chloride, 8-10 parts of triallylamine, 2-5 parts of organo-siloxane, 3-5 parts of glacial acetic acid, 0.1-1 part of azodiisobutyronitrile and 100-120 parts of deionized water. The fabric formaldehyde-free fixing agent is simple in preparation process, the prepared fixing agent is free of formaldehyde and APEO (Alkylphenol Ethoxylates), static combination of cation groups in fixing agent molecules with anion groups in dye can be achieved, insoluble lake can be formed on the surface of a fabric, and hydrosolvent groups of the dye are sealed up, so that the washing fastness of the colored fabric can be improved.

Description

technical field [0001] The invention belongs to the technical field of textile auxiliaries, and in particular relates to an formaldehyde-free color-fixing agent for fabrics and a preparation method thereof. Background technique [0002] In the process of fabric weaving, although some dyes are brighter in color, due to the poor fastness of wet treatment, the phenomenon of fading and sticking is more serious, which not only makes the fabric itself look old, but also easily fades when it meets water. It is easy to cause mutual staining with other fabrics. [0003] Fixing agent is an auxiliary agent used to improve the color fastness of dyes on fabrics to wet treatment. It can form insoluble colored matter with dyes on fabrics to improve the color fastness to washing and perspiration, and sometimes to improve its light fastness. Traditional color fixing agents contain harmful substances such as formaldehyde, but with the improvement of economic level, people have higher and hi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/52D06P1/653D06P1/48C08F291/12C08F226/02C08F220/34C08F220/16C08F230/08C08F4/04
Inventor 朱卫强
Owner JIANGSU ZHONGXIN RESOURCES GRP
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