Materials for electronic devices

A technology of atoms and macromolecules, applied in the direction of electric solid-state devices, luminescent materials, electrical components, etc., can solve the problems of limited organic electroluminescent devices

Active Publication Date: 2014-04-09
MERCK PATENT GMBH
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  • Abstract
  • Description
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  • Application Information

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Problems solved by technology

In particular, the properties of the host material often limi...

Method used

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Experimental program
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Embodiment

[0225] Synthesis of compounds 1 to 13 of the present invention

[0226] Unless otherwise specified, the following syntheses were carried out under a protective gas atmosphere. Starting materials can be purchased from ALDRICH or ABCR (palladium(II) acetate, tri-o-tolylphosphine, inorganics, solvents). 3-bromofluorenone (Tetrahedron (tetrahedron), 51, 7, 2039-54; 1995) and 3-bromofluorene and the synthesis of bis-biphenyl-4-yl-(4'-bromobiphenyl-4-yl)amine (JP2010-111605).

[0227] Precursor A: 3-bromo-9H-fluorene

[0228]

[0229] To a vigorously stirred and refluxed suspension of 64 g (250 mmol) of 3-bromofluorene in a mixture of 1000 ml of toluene and 2000 ml of ethanol was added 49 ml (1000 mmol) of hydrazine hydrate followed by 3 g of freshly prepared Raney nickel. After reflux for 2 hours, the mixture was cooled, the solvent was removed in vacuo, the residue was dissolved in 1000ml of warm chloroform, the solution was filtered through silica gel, the clear solution wa...

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Abstract

The invention relates to a compound of formula (I), (II) or (III), to the use of the compound in an electronic device, and to an electronic device containing a compound of formula (I), (II) or (III). The invention further relates to a method for producing a compound of formula (I), (II) or (III) and to a formulation containing one or more compounds of formula (I), (II) or (III).

Description

technical field [0001] The present invention relates to compounds of formula (I), (II) or (III), to the use of said compounds in electronic devices, and to electronic devices comprising compounds of formula (I), (II) or (III). The invention also relates to processes for the preparation of compounds of formula (I), (II) or (III), and to formulations comprising one or more compounds of formula (I), (II) or (III). Background technique [0002] The development of functional compounds for use in electronic devices is the subject of intense current research. The aim here is in particular to develop compounds with which improvements in the properties of electronic devices, such as power efficiency, lifetime or color coordinates of the luminescence, can be obtained at one or more relevant points. [0003] According to the present invention, the term electronic device is in particular taken to mean organic integrated circuits (OICs), organic field-effect transistors (OFETs), organic...

Claims

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Application Information

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IPC IPC(8): H01L51/00C09K11/06
CPCH01L51/0061H01L51/006H01L51/0035C09K11/06H01L51/0073H01L51/0072Y02E10/549H01L51/0074H10K85/636H10K85/633H10K85/6576H10K85/6574H10K85/6572C09K2211/1007C09K2211/1011C09K2211/1014C09K2211/1029C09K2211/1033C09K2211/1088C09K2211/1092C07C255/58C07C209/10C07C211/61C07D403/04C07D209/86C07C2603/18C07C2603/94C07C211/54C07D209/82H10K99/00H10K85/111
Inventor 埃米尔·侯赛因·帕勒姆阿尔内·比辛克里斯托夫·普夫卢姆特雷莎·穆希卡-费尔瑙德菲利普·斯托塞尔托马斯·埃伯利弗兰克·福格斯
Owner MERCK PATENT GMBH
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