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A kind of industrialized production preparation process of glycine chelated manganese

A glycine chelated manganese, preparation technology, applied in the preparation of organic compounds, cyanide reaction preparation, organic chemistry, etc., to achieve the effect of simple synthesis route, short reaction cycle, safe and reliable process

Active Publication Date: 2015-12-30
山东祥维斯生物科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] However, the inventor has found in actual work that when the above two methods are used for production, two substances, manganese glycinate and manganese hydroxide, will exist in the product, and neither glycine nor manganese salt has reacted completely

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0028] A kind of industrialized production preparation process of glycine chelated manganese, the steps are as follows:

[0029] (1) Put 400kg of manganese sulfate monohydrate into the 2000L reaction kettle, inhale 800kg of pure water, start stirring, raise the temperature to 40°C to completely dissolve, add 620kg of 32wt% sodium hydroxide solution under 0.01MPa vacuum to generate hydrogen Manganese oxide white solid, reacted for 0.5h after dropping;

[0030] (2) Cool down to 20°C, centrifugally filter, and use a double-cone vacuum dryer to dry at 60°C for 4 hours at a vacuum degree of 0.06MPa;

[0031] (3) Take 180kg of dried solids, put them into a 2000L reactor, inhale 400kg of pure water, start stirring, control the vacuum at 0.01MPa, and raise the temperature to 40°C;

[0032] (4), 300kg glycine is dissolved in 800kg water to make glycine solution;

[0033] (5) Add 1kg of sulfuric acid to the 2000L reactor, open the head tank valve and add the glycine solution dropwise ...

Embodiment 2

[0041] A kind of industrialized production preparation process of glycine chelated manganese, the steps are as follows:

[0042] (1) Put 420kg of manganese sulfate monohydrate into a 2000L reactor, inhale 850kg of pure water, start stirring, raise the temperature to 50°C to completely dissolve, add 650kg of 32wt% sodium hydroxide solution under 0.01MPa vacuum to generate hydroxide Manganese white solid, react for 1h after dropping;

[0043] (2) Cool down to 20°C, centrifugally filter, use double-cone vacuum dryer, vacuum degree 0.10MPa, dry at 60°C for 5h;

[0044] (3) Take 180kg of dried solids, put them into a 2000L reactor, inhale 500kg of pure water, start stirring, control the vacuum at 0.01MPa, and raise the temperature to 50°C;

[0045] (4), 320kg glycine was dissolved in 800kg water to make glycine solution;

[0046] (5) Add 5kg of sulfuric acid to the 2000L reactor, open the head tank valve and add the glycine solution dropwise to the 2000L reactor, keep the tempera...

Embodiment 3

[0054] A kind of industrialized production preparation process of glycine chelated manganese, the steps are as follows:

[0055] (1) Put 410kg of manganese sulfate monohydrate into a 2000L reactor, inhale 830kg of pure water, start stirring, raise the temperature to 45°C to completely dissolve, add 635kg of 32wt% sodium hydroxide solution under 0.01MPa vacuum to generate hydrogen oxide Manganese white solid, reacted for 0.8h after dropping;

[0056] (2) Cool down to 20°C, centrifugally filter, use double-cone vacuum dryer, vacuum degree 0.08MPa, dry at 60°C for 4.5h;

[0057] (3) Take 180kg of dried solids, put them into a 2000L reactor, inhale 450kg of pure water, start stirring, control the vacuum at 0.01MPa, and raise the temperature to 45°C;

[0058] (4), 310kg glycine was dissolved in 800kg water to make glycine solution;

[0059] (5) Add 3kg of sulfuric acid to the 2000L reactor, open the head tank valve and add the glycine solution dropwise to the 2000L reactor, keep th...

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Abstract

A kind of industrial production preparation process of glycine chelated manganese, the steps are as follows: Manganese sulfate monohydrate is mixed with sodium hydroxide solution under certain conditions to form manganese hydroxide white solid, filtered and dried, then sulfuric acid is added, and glycine solution is added dropwise to react After the reaction is completed, the filtrate is concentrated for 2-4 hours at a vacuum degree of 0.07 MPa or more, and 60-70 parts by weight of acetone is added to the solution to precipitate a solid; centrifugal filtration, using a double-cone vacuum dryer, and drying at a vacuum degree of 0.06 MPa or more at 80°C for 2 hours to 3 hours , to obtain glycine chelated manganese products. The invention has the advantages of simple synthesis route, safe and reliable process, short reaction cycle, high yield, good product quality and no pollutant generation.

Description

technical field [0001] The invention relates to a preparation process suitable for the industrial production of glycine chelated manganese. Background technique [0002] Trace elements are one of the essential nutrients for animals to maintain life and produce, directly participate in almost all physiological and biochemical functions of the body, and play an extremely important role in life activities. Trace element additives have gone through three stages of development: inorganic salt additives, simple organic matter and trace element amino acid chelates. Trace element amino acid chelate, as the third generation trace element, is regarded as an ideal trace element because of its good chemical stability, high biological effect, easy digestion, anti-interference, non-toxic and non-irritating characteristics. Elemental supplements. [0003] Manganese is one of the indispensable trace elements for animal growth, reproduction and a series of life activities, and plays an imp...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07C229/76C07C227/18
Inventor 马兴群丁振柱张毅丰张守伟胡发明
Owner 山东祥维斯生物科技股份有限公司
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