New lung-oncocyte-apoptosis inducing fusion protein and application thereof
A fusion protein and tumor cell technology, applied in peptide/protein components, medical preparations containing active ingredients, hybrid peptides, etc., can solve the problems of lung tumor cell apoptosis
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Embodiment 1
[0045] Example 1: Preparation of EGFR (L858R) mutant-specific mouse monoclonal antibody.
[0046] Artificial chemical synthesis of EGFR (L858R) mutant-specific short peptide, the short peptide sequence is TDFGRAKKLLGGGC. The EGFR (L858R) short peptide was covalently cross-linked with the KLH carrier protein using the C amino acid residue at the end of the short peptide (Kit from Thermo Scientific, product number #77605). The preparation method of the hybridoma secreting monoclonal antibody in the present invention is carried out according to Harlow, E & Lane, D: Antibodies: A Laboratory Manual; Cold Spring Harbor Laboratory Press, 1988, unless otherwise specified. The cross-linked product was used to immunize Balb / c mice with Freund's complete adjuvant and Freund's incomplete adjuvant, and the antigen dose for each immunization was 0.5 mg. After three immunizations, when the EGFR (L858R) specific antibody titer in the serum reached 1:10000, the mouse spleen cells were fused w...
Embodiment 2
[0047] Example 2: Preparation of heavy chain and light chain variable regions of humanized EGFR (L858R) mutant mouse monoclonal antibody
[0048]In order to clone the cDNA encoding antibody VH and VL from hybridoma cells (4G8) that secrete specific monoclonal antibodies that recognize human EGFR (L858R) mutants, first follow the method published by Zhou et al. (Zhou, H. et al: Nucleic Acids Res22:888-9, 1994), synthesized a set of universal (universal) oligonucleotide primers for cloning mouse VH and VL cDNA. Total RNA was extracted from 5×106 hybridoma (4G8) cells as a template, and oligo (dT) was used as a primer to catalyze the synthesis of cDNA under the action of ligase. The cDNA synthesis reaction mediated by reverse transcriptase is as follows:
[0049]
[0050] Reaction environment: 30°C, 10 minutes; 50°C, 30 minutes; 95°C, 5 minutes; store at 4°C for later use.
[0051] Further, the cDNA synthesized by the reverse transcription reaction was used as a template, an...
Embodiment 3
[0055] Example 3: Expression and preparation of VH-GGG-Apaf-1 (1-97aa)-9R fusion protein (SBC-426) in Escherichia coli
[0056] According to the VH-GGG-Apaf-1 (1-97aa)-9R amino acid sequence and the codon preference of Escherichia coli, the optimized DNA sequence encoding the fusion protein suitable for expression in Escherichia coli was artificially synthesized. When synthesizing the gene, a KpnI restriction site GGTACC was introduced at its 5' end, and a stop codon TAA and a SalI restriction site GTCGAC were introduced at its 3' end. The following molecular cloning operation methods, unless otherwise specified, refer to the literature: Green.M.R: Molecular cloning, A Laboratory Manual (4th), Cold Spring Harbor Press, 2012. The synthetic DNA sequence was first cloned into pBluescript (+ ) plasmid to hold the synthetic DNA sequence. Further, the gene encoding the fusion protein was excised from pBluescript (+) plasmid with KpnI and SalI and cloned into pET32a (+) expression v...
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