Preparation method of graphene film

A graphene film and film technology, applied in graphene, nano-carbon and other directions, can solve the problems of waste of resources, complicated preparation process of graphene wave film, human and environmental damage, etc.
CN103754864AInactive Publication Date: 2014-04-30UNIV OF SHANGHAI FOR SCI & TECH

Patent Information

Authority / Receiving Office
CN · China
Patent Type
Applications(China)
Current Assignee / Owner
UNIV OF SHANGHAI FOR SCI & TECH
Publication Date
2014-04-30
Estimated Expiration
Not applicable · inactive patent

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Abstract

The invention discloses a preparation method of a graphene film. The preparation method comprises the steps: firstly, dissolving polymethyl methacrylate into acetone to obtain a polymethyl methacrylate and acetone liquid; then, dropwise adding the polymethyl methacrylate and acetone liquid on a metal to form a layer of polymethyl methacrylate film; covering a quartz glass slide on the polymethyl methacrylate film; then, simultaneously placing the metal sheet, the polymethyl methacrylate film on the metal sheet and the covered quartz glass slide into a high-temperature annealing furnace with a nitrogen condition, and carrying out high-temperature annealing while controlling the temperature at 800-1000 DEG C, wherein the polymethyl methacrylate is decomposed into a graphene film under the catalytic action of the metal in the metal film, and the graphene film is evaporated at a high temperature and is transferred on the quartz glass slide; and next, naturally cooling to room temperature to obtain a layer of graphene film on the quartz glass slide. The preparation method disclosed by the invention is simple and convenient to implement and capable of transferring graphene under the condition that the graphene is not damaged or polluted.
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Description

technical field

[0001] The invention relates to a preparation method of a graphene film, in particular to a preparation method of an in-situ metal catalytic decomposition and transfer of a graphene film, specifically involving the preparation of graphene by metal in-situ decomposition, and finally transferring the graphene by thermal evaporation To the target substrate, so that the graphene can be directly transferred to the target substrate without intermediate treatment. Background technique

[0002] Graphene is a new type of transparent conductive film material. The transmittance of visible light of single-layer graphene is as high as 97.7%. It also has good electrical conductivity, flexibility and mechanical strength. Due to its superior optical and electrical properties, it has attracted more and more attention in the fields of scientific research and engineering applications. At present, it has been widely used in micro-nano electronic devices, electronic energy stora...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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