Method for preparing geniposide in eucommia leaf
A technology of geniposide and Eucommia ulmoides leaves is applied in the field of preparing geniposide from Eucommia ulmoides leaves, which can solve the problems of large amount of waste water, low product purity, low extraction rate and the like, and achieves low water extraction temperature and simple membrane operation process. , the effect of shortening the extraction time
Inactive Publication Date: 2014-05-14
HUBEI LAOLONGDONG DUZHONG DEV
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The invention discloses a method for preparing geniposide in eucommia leaf. The method comprises the following steps of crushing eucommia leaf, carrying out cellulase-assistant middle temperature-water extraction, carrying out routine filtration, carrying out ultrafilter membrane impurity-removal, carrying out nanofiltration condensation, carrying out macroporous resin-based separation purification, carrying out condensation and carrying out drying to obtain geniposide powder. The method utilizes cellulase-assistant middle temperature-water extraction of geniposide in eucommia leaf, has an extraction rate of 95%, a low water extraction temperature and short extraction time, utilizes an ultrafilter membrane to remove impurities and separate other side products in the extract, has simple membrane processes and realizes long-term membrane flux stabilization, easy membrane cleaning, a long service life and industrialization. Through the nanofiltration membrane, the extract subjected to impurity removal is concentrate d so that follow-up technical load is reduced and a resin service life is prolonged. Through the method, a nanofiltrated liquid has a COD value <=100 and can be reused in production and basically, waste water is not produced. Through the macroporous adsorption resin, geniposide can be effectively purified. The powder produced by the method has geniposide purity greater than 80% and an extraction rate more than 1.2%.
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