Preparation method for spiral-wound ultrafiltration membrane with low molecular weight cut off as well as product thereof
An ultrafiltration membrane, molecular weight technology, applied in chemical instruments and methods, membrane technology, semi-permeable membrane separation, etc., to achieve the effect of convenient process control, simple molding procedure and good simplicity
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Embodiment 1
[0029] Mix 25 parts of polysulfone (polymer), 3 parts of additives (among them, additives include 1 part of anhydrous lithium chloride and 2 parts of propanol), and 79 parts of dimethylacetamide (solvent) at 80 ° C Uniformly mixed and dissolved under the temperature conditions, and the film-making liquid was obtained after filtering and defoaming in a conventional way.
[0030] Install the polyester non-woven fabric as the supporting layer on the film scraping machine, adjust the thickness of the scraper and the cloth speed of the linear speed controller, and pour the pre-prepared film-making solution into the film-making solution storage tank slowly and steadily. Start the scraping machine, and the film-making solution is coated and scraped on the polyester non-woven fabric. After an air exposure distance of 15cm, it is immersed in a constant temperature coagulation bath at 6°C, and then fully rinsed through the rinsing tank to obtain ultrafiltration with a low molecular weigh...
Embodiment 2
[0034] 20 parts of polyethersulfone (polymer), 4 parts of additives (among them, additives include 2 parts of phosphoric acid and 2 parts of propanol), 76 parts of dimethylformamide (solvent) at a temperature of 70 ° C Mix and dissolve evenly under the environment, filter and defoam in a conventional way to obtain the film-making liquid.
[0035] Install the polyester non-woven fabric as the supporting layer on the film scraping machine, adjust the thickness of the scraper and the cloth speed of the linear speed controller, and pour the pre-prepared film-making solution into the film-making solution storage tank slowly and steadily. Start the scraping machine, and the film-making solution is applied and scraped on the polyester non-woven fabric. After an air exposure distance of 10cm, it is immersed in a constant temperature coagulation bath at 8°C, and then fully rinsed through the rinsing tank to obtain ultrafiltration with a low molecular weight cut-off. Diaphragm.
[0036...
Embodiment 3
[0039] 16 parts of polyvinylidene fluoride (polymer), 8 parts of additives (among them, additives include 3 parts of polyvinylpyrrolidone and 5 parts of acetone), 76 parts of N-methylpyrrolidone (solvent) at 75 ° C Mix and dissolve evenly under temperature conditions, filter and defoam in a conventional way to obtain a film-forming solution.
[0040] Install the polyester non-woven fabric as the supporting layer on the film scraping machine, adjust the thickness of the scraper and the cloth speed of the linear speed controller, and pour the pre-prepared film-making solution into the film-making solution storage tank slowly and steadily. Start the scraping machine, and the film-making solution is applied and scraped on the polyester non-woven fabric. After an air exposure distance of 10cm, it is immersed in a constant temperature coagulation bath at 8°C, and then fully rinsed through the rinsing tank to obtain ultrafiltration with a low molecular weight cut-off. Diaphragm.
[...
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Abstract
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