Polyether modified organic silicon defoamer and preparation method thereof
A technology of silicone defoamer and polyether modified silicone oil, which is applied in textiles, papermaking, fiber processing, etc., can solve the problems of high price, short foam suppression time, low surface energy, etc., and achieves simple manufacturing method and foam suppression. Long time, increased dispersion effect
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Embodiment 1
[0023] The weight percentage composition of the compounded raw materials of the polyether modified silicone defoamer is: 10% polyether modified silicone oil, 15% white carbon black, 25% dimethyl silicone oil, 9% emulsifier, 4% regulator, Water 37%. Emulsifier is Span60, regulator is C 4 Fatty alcohol polyoxyethylene ether. The preparation process is:
[0024] (a) Put polyether modified silicone oil, white carbon black and dimethyl silicone oil into the reaction kettle by weight percentage, stir and heat up to 200°C to prepare silicone paste;
[0025] (b) Add the emulsifier Span60 into the silicone paste, heat it to 50°C, and then add the modifier C 4 Fatty alcohol polyoxyethylene ether, add water drop by drop, stir for 8 hours, cool, discharge, and pack.
Embodiment 2
[0027] The weight percentage composition of the compounded raw materials of the polyether modified silicone defoamer is: 10% polyether modified silicone oil, 10% white carbon black, 40% dimethyl silicone oil, 9% emulsifier, 3% regulator, Water 28%. The emulsifier is Span60 and Tween60, the regulator is C 4 Fatty alcohol polyoxyethylene ether. The preparation process is:
[0028] (a) Put polyether modified silicone oil, white carbon black and dimethyl silicone oil into the reaction kettle by weight percentage, stir and heat up to 200°C to prepare silicone paste;
[0029] (b) Add the emulsifier (the weight ratio of Span60 and Tween60 is 1:1) into the silicone paste, heat it to 50°C, and then add the modifier C 4 Fatty alcohol polyoxyethylene ether, add water drop by drop, stir for 8 hours, cool, discharge, and pack.
Embodiment 3
[0031] The weight percentage composition of the compounded raw materials of the polyether modified silicone defoamer: 5% polyether modified silicone oil, 15% white carbon black, 30% dimethyl silicone oil, 10% emulsifier, 1.75% regulator, Water 38.25%. The emulsifier is Span40, Span60 and Tween60, and the regulator is C 4 Fatty alcohol polyoxyethylene ether. The preparation process is:
[0032] (a) Put polyether modified silicone oil, white carbon black and dimethyl silicone oil into the reaction kettle by weight percentage, stir and heat up to 200°C to prepare silicone paste;
[0033] (b) Dissolve the emulsifier (the weight ratio of Span40, Span60 and Tween60 is 1:2:2) at 70°C and add it to the silicone paste, heat it to 75°C, and then add the modifier C 4 Fatty acid polyoxyethylene ether, add water drop by drop, stir for 7 hours, cool, discharge, and pack.
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