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76results about How to "Long foam suppression time" patented technology

Preparation method of defoaming agent for waterborne system

The invention relates to a preparation method of a defoaming agent for a waterborne system. The preparation method of the defoaming agent for the waterborne system comprises the following steps: a) adding silicon oil, gaseous silicon dioxide and catalyst into a reaction container according to proportions, and preparing silicon cream under an agitating condition protected by nitrogen; b) adding hydrogen-containing silicon oil and allyl polyether into the reaction container, agitating under the protection of nitrogen, increasing temperature and adding an initiator for reaction to obtain polyether modified organic silicon; c) jading the silicon cream obtained in step a), the polyether modified organic silicon obtained in step b) and an emulsifier into the reaction container, adding water for emulsification under a high-speed agitating condition, and adding a thickening agent to regulate viscosity to obtain a product. The defoaming agent prepared by adopting the preparation method provided by the invention has the advantages that the active components are low, the manufacturing cost is low and the environmental friendliness is better; the emulsification is stable, the compatibility in the waterborne system is good, the defoaming agent is easy to disperse, the surface tension is low, the defoaming speed is quick, the foam inhibiting time is long, the thermal resistance, shear resistance and acid and alkali resistance thereof are good, and the defoaming agent can adapt to various places; the defoaming agent can be separately used and can also be jointly used with other adjuvants, the stability is good, the phenomenon of oil floating due to demulsification does not occur, no sediment is produced and shrinkage cavities during coating are not caused; and the defoaming agent is also very effective to non-waterborne systems.
Owner:KITO CHEM CO LTD

Self-emulsifying molecular antifoaming agent and preparation method thereof

The invention discloses a self-emulsifying molecular antifoaming agent and a preparation method thereof. The antifoaming agent comprises the following components in percent by mass: 20 to 60 percent of antifoaming active substance and 40 to 80 percent of dispersion medium, wherein the antifoaming active substance consists of higher fatty alcohol, alkynol, polyether and silicone oil in a mass ratio of 1:(0.8-1.5):(2-3):(2-4); and the dispersion medium is grafted star polymer. The preparation method comprises the following steps of: adding 50 to 150 parts of trichloromethane and 1 to 2 parts ofp-methyl benzene sulfonic chloride into 20 to 60 mass parts of active substance and 40 to 80 mass parts of star polymer, raising the temperature to between 40 and 70 DEG C, and reacting for 3 to 6 hours; and after the reaction is finished, washing sodium carbonate until the ph is 7, drying by using anhydrous sodium sulfate, and evaporating the solvent under reduced pressure to obtain the antifoaming agent. The extended arm of the star polymer in the antifoaming agent is grafted with the active substance, so that various components are synergistic, and the obtained antifoaming agent is high instability, low in surface tension, high in surface activity, high in antifoaming capacity, long in foam inhibition time and small in dosage.
Owner:JINHU JINLING NEW MATERIAL SCI & TECH

Polyether modified organic silicon defoamer safe to strains and preparation method thereof

The invention belongs to the technical field of defoamers and discloses a polyether modified organic silicon defoamer safe to strains and a preparation method thereof. The preparation method includesthe following steps that: silicon dioxide nanometer microspheres, dimethyl silicone oil, DMF and deionized water are sequentially added into a reaction flask, ammonia water is added while stirring isconducted, heating is conducted to 50-70 DEG C, a reaction is conducted for 1-2 hours, cooling is conducted to the room temperature, and centrifugation is conducted, a precipitate is washed with ethanol, and drying is performed to obtain dimethicone grafted and modified silicon dioxide nano microspheres; 30-60 parts of the dimethicone grafted and modified silicon dioxide nano microspheres, 30-50 parts of polyether modified silicon oil, 1-10 parts of a thickener, 2-10 parts of an emulsifier and 10-50 parts of water are added into a dispersion tank, heating is conducted to 180-200 DEG C, stirring is performed for 2-3 hours, gradient cooling is carried out to 50-60 DEG C in a stirring state, and finally natural cooling is performed to obtain the polyether modified organic silicon defoamer. The defoamer has the advantages of being low in surface tension, high in defoaming speed, long in foam inhibition time, small in dosage, free of toxicity and harm to strains, wide in application range and the like.
Owner:JIANGSU SAIOUXINYUE DEFOAMER

Preparation method of high-molecular-weight block polyether, silyl ether mixed defoaming agent and preparation method thereof

The invention provides a silyl ether mixed defoaming agent. The silyl ether mixed defoaming agent comprises the following components in parts by weight: 24-40 parts of high molecular weight block polyether; 20-30 parts of polymer polyether modified polysiloxane; 10-30 parts of fatty alcohol; and 15-35 parts by weight of a cosolvent; wherein the high-molecular-weight block polyether is obtained bypolymerizing polyol and alkylene oxide; wherein the high-molecular silyl ether modified polysiloxane is prepared from high-molecular-weight block polyether modified polysiloxane. Compared with the prior art, the polyether chain segment with hydrophilicity is grafted to the polysiloxane chain segment with hydrophobicity, so that the formed silyl-ether copolymer has the advantages of two defoaming agents, namely silicon and ether; the high molecular polyether modified polysiloxane and the high molecular weight block polyether are compounded for use, so that the good defoaming effect of the highmolecular polyether modified polysiloxane and the good foam inhibition effect of the high molecular weight block polyether have a synergistic effect, the reduction of the foam amount is effectively ensured, and meanwhile, the fatty alcohol with high surface activity is matched, so that the improvement of the defoaming efficiency is promoted.
Owner:SHANDONG EFIRM BIOCHEMISTRY & ENVIRONMENTAL PROTECTION CO LTD

Water body-oriented low-COD defoaming agent non-toxic to microorganisms and preparation method of defoaming agent

The invention belongs to the technical field of chemical additives, and particularly discloses a water body-oriented low-COD defoaming agent non-toxic to microorganisms and a preparation method of thedefoaming agent. The defoaming agent is prepared from the following components in parts by weight: 10-20 parts of polydimethylsiloxane, 20-40 parts of mineral oil, 20-40 parts of amino silicone oil modified epoxy castor oil, 1-10 parts of hydrophobic white carbon black, 0.5-5 part of a defoaming aid and 0.1-10 part of an emulsifier.The preparation method comprises the following steps of: adding the epoxy castor oil and amino silicone oil into an organic solvent; adding a basic catalyst; performing stirring for reaction for 8-12 hours at the temperature of 60-80 DEG C; performing centrifugingto obtain supernatant; and carrying out rotary evaporation to remove the organic solvent, thereby obtaining the silicone oil modified epoxy castor oil. The defoaming agent disclosed by the invention is good in chemical stability, small in dosage, high in defoaming speed, long in foam inhibition time, high in efficiency, non-toxic to microorganisms and easy to disperse in sewage, and can reduce thesurface tension of a foam film, quickly eliminate foam and solve the problem of foam generated by biochemical sewage treatment.
Owner:JIANGSU SAIOUXINYUE DEFOAMER
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