Defoaming agent
A defoamer and catalyst technology, applied in the direction of foam dispersion/prevention, chemical instruments and methods, liquid degassing, etc., can solve the problems of product and equipment impact, impact on defoaming performance, oil floating, etc. The effect of long soaking time and strong defoaming ability
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[0080] The second aspect of the present invention provides a kind of preparation method of defoamer, and described preparation method comprises the following steps:
[0081] (1) Preparation of organosilicon composition:
[0082] Mix and stir silicone oil and MQ silicone resin, heat to 110-170°C, add white carbon black, keep warm at 130-190°C for 1.5-5.5h, and wait until the temperature drops to 35-50°C to obtain the product.
[0083] (2) Preparation of defoamer:
[0084] Mix the silicone composition, hydrogen-containing polysiloxane, vinyl polysiloxane, and allyl polyether evenly, raise the temperature to 60-70°C, then add the catalyst, raise the temperature to 90-110°C, and set the temperature at 250-350rpm React for 0.5~1.0h under stirring condition; cool down to 70~75℃, add emulsifier and preservative, mix under stirring condition of 250~350rpm for 0.3~0.6h; 0.3 ~ 0.6h, and keep the temperature at 70 ~ 75 ℃, that is.
[0085] In a preferred embodiment, the concentration ...
Embodiment 1
[0090]Example 1 provides a defoamer. In parts by weight, the preparation raw materials include at least: 20 parts of silicone composition, 5 parts of hydrogen-containing polysiloxane, 5 parts of vinyl polysiloxane, allyl polysiloxane 6 parts of ether, 1 part of catalyst, 10 parts of emulsifier, 2 parts of thickener, 2 parts of preservative, 70 parts of water.
[0091] The silicone composition is a combination of silicone oil, hydrophobic white carbon black, and MQ silicone resin, wherein the weight ratio of white carbon black, silicone oil, and MQ silicone resin is 1:18:2.
[0092] The silicone oil is a composition of dimethyl silicone oil and hydroxy silicone oil, wherein the mass ratio of dimethyl silicone oil and hydroxy silicone oil is 3.5:1.
[0093] The viscosity of the simethicone oil is 50000mPa·s (25°C), and the purchaser is Jinan Xushun Chemical Co., Ltd.
[0094] The hydroxyl mass percentage of the hydroxy silicone oil is 3.8%, and the purchaser is Guangzhou Putai ...
Embodiment 2
[0110] Example 2 provides a defoamer. In parts by weight, the preparation raw materials include at least: 10 parts of silicone composition, 1 part of hydrogen-containing polysiloxane, 1 part of vinyl polysiloxane, allyl polysiloxane 2 parts ether, 0.1 part catalyst, 5 parts emulsifier, 1 part thickener, 1 part preservative, 50 parts water.
[0111] The silicone composition is a combination of silicone oil, hydrophobic white carbon black, and MQ silicone resin, wherein the weight ratio of white carbon black, silicone oil, and MQ silicone resin is 1:18:2.
[0112] The silicone oil is a composition of dimethyl silicone oil and hydroxy silicone oil, wherein the mass ratio of dimethyl silicone oil and hydroxy silicone oil is 3.5:1.
[0113] The viscosity of the simethicone oil is 50000mPa·s (25°C), and the purchaser is Jinan Xushun Chemical Co., Ltd.
[0114] The hydroxyl mass percentage of the hydroxy silicone oil is 3.8%, and the purchaser is Guangzhou Putai New Material Co., Lt...
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