Epoxy resin-base film for flexible or thin-film solar cells and preparation method thereof
A technology of epoxy resin base film and solar cell, which is applied in the direction of circuits, photovoltaic power generation, electrical components, etc., can solve the problem of low shrinkage, achieve the effect of improving power generation efficiency and light absorption efficiency
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Embodiment 1
[0024] (1) 8Kg glycidyl ether epoxy resin solution (solid content of epoxy resin is 10%) (Zhejiang Kaihua Chengxin Resin Co., Ltd.), 20 Kg N,N-dimethylformamide, 10Kg toluene to prepare a solution , the epoxy resin-based solution; 61.9999 Kg tetrahydrofuran was stirred and blended evenly at a temperature of 0°C with an emulsifier;
[0025] (2) Add 0.0001Kg nano-aluminum powder to the above solution at room temperature and mix it with an emulsifier, and use ultrasonic treatment to obtain a uniformly mixed colloidal blend;
[0026] (3) Import the above blend into the screw mixing extruder for blending and extrusion, the temperature is controlled at 80-90 ° C, the extruded product is filtered through a 150-mesh filter, the pressure difference between the inlet and outlet of the metering pump is 1 MPa, metered, extruded, and cast A film thickness of 100 UM, 10 degrees air cooling, 2 times the drafting ratio drawing, pulling, coiling and other processes, to obtain a flexible or thi...
Embodiment 2
[0029] (1) Mix 9Kg glycidyl ester epoxy resin solution (solid content of epoxy resin is 8%) (Foshan Longxiang Resin Raw Materials Co., Ltd.), with 10 Kg N,N-dimethylformamide, 10Kg acetone, 10Kg tetrahydrofuran and 10Kg butyl acetate were prepared into a solution; the epoxy resin-based solution; 50.9Kg tetrahydrofuran was stirred and blended evenly at a temperature of 140°C with an emulsifier;
[0030](2) Add 0.1Kg of nano-aluminum powder to the above solution at room temperature and mix it with an emulsifier, and use ultrasonic treatment to obtain a uniformly mixed colloidal blend;
[0031] (3) Import the above blend into a screw mixing extruder for blending and extrusion, the temperature is controlled at 80°C, the extrudate is filtered through a 150-mesh filter, the pressure difference between the inlet and outlet of the metering pump is 1MPa, metered and extruded, and the cast film thickness 100UM, 10 degrees air cooling, 2 times the drafting ratio, drawing, pulling, coilin...
Embodiment 3
[0034] (1) Mix 10Kg glycidylamine epoxy resin solution (solid content of epoxy resin is 5%) (Foshan Longxiang Resin Raw Material Co., Ltd.), with 10 Kg N,N-dimethylformamide, 10Kg benzene, 10Kg tetrahydrofuran and 10Kg butyl acetate were prepared into a solution, and the epoxy resin-based solution and 49.999% benzene were stirred and blended evenly at a temperature of 100°C with an emulsifier;
[0035] (2) Add 0.001Kg nano-aluminum powder to the above solution at room temperature and mix it with an emulsifier, and use ultrasonic treatment to obtain a uniformly mixed colloidal blend;
[0036] (3) Import the above blend into a screw mixing extruder for blending and extrusion, the temperature is controlled at 90°C, the extrudate is filtered through a 150-mesh filter, the pressure difference between the inlet and outlet of the metering pump is 1MPa, metered and extruded, and the cast film thickness 100UM, 10 degrees air cooling, 2 times the drafting ratio, drawing, pulling, coilin...
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