Silk fibroin cartilage complex artificial ear and preparation method thereof
A complex and silk fibroin technology, applied in prosthetics, medical science, etc., to achieve the effect of promoting epithelial crawling, good biocompatibility, and promoting cell growth
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[0051] 1) Preparation of silk fibroin
[0052] Use waste mulberry silkworm raw silk to degummed in NaHCO3 (0.5wt%) aqueous solution, dissolve the degummed silk in 9.3mol / L LiBr aqueous solution, stir until the silk is completely dissolved, filter, remove undissolved silk and impurities, and obtain silk fibroin Salt solution, remove the LiBr in the solution by dialysis with deionized water, get the silk protein that concentration is 4%, concentrate again, PEG dialysis, the centrifugation of gained silk fibroin solution removes impurity, stay supernatant, the silk fibroin concentration of gained is 10%, store in a 4°C refrigerator for later use;
[0053] 2) Preparation of silk fibroin scaffold
[0054] Mix the prepared silk fibroin solution with n-butanol 1:1, stir for 5 minutes (25°C), put into a 5cm×5cm polystyrene disk, then put it into a -20°C refrigerator for 24 hours, at room temperature, The preparation of the silk fibroin porous scaffold is completed; then the residual...
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