Silver-coated hollow bead compound filament yarn antibiosis fiber and preparation method thereof
A technology of hollow microbeads and composite filaments, which is applied in the manufacture of rayon, fiber chemical characteristics, and single-component polyolefin rayon, etc., and can solve the problem of expensive nano-silver antibacterial fibers and large particle sizes of silver-coated hollow microbeads and other problems, to achieve the effects of high efficiency and broad-spectrum antibacterial properties, cost reduction, and improved dispersion
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[0032] The preparation method of the dispersant of the embodiment of the present invention is: mixing polyvinyl alcohol, glycerin and polyvinyl pyrrolidone, stirring at 40-50°C for 30-60 minutes, and drying at 90°C.
[0033] The determination method of the silver-plated hollow microsphere composite filament antibacterial fiber of the present invention adopts national standard GB / T3916-1997 "the determination of breaking strength and elongation at break of single yarn of textile package yarn" ".
[0034] Test method: Take the prepared antibacterial fiber filament section and take a sample with a length of more than 500mm. After adjusting the humidity, clamp it into the holder of the test instrument, so that the distance between the upper and lower holders is 500mm, and then start the instrument. The interval length was stretched at a speed of 500 mm / min until it broke, and the breaking strength was recorded in cN / dtex; the percentage of the increased length at break and the cla...
Embodiment 1
[0036] The preparation steps of the 50 / 50 side-by-side silver-plated hollow microsphere composite filament antibacterial fiber are as follows:
[0037] (1) Component B is made of the following raw materials in parts by weight: silver-plated hollow microspheres 16, dispersant 14, and polypropylene (PP) high polymer chip powder 70.
[0038] Wherein the dispersant is made of the following raw materials in parts by weight: polyvinyl alcohol 11.2, glycerin 2.1, polyvinylpyrrolidone 0.7.
[0039] The preparation method of component B: fully stir and mix the silver-plated hollow microspheres and the dispersant, and use a high-speed shear mixer to mix the mixed materials evenly to obtain a composite powder. Mix the above composite powder and PP high polymer chip powder evenly with a mixer, vacuumize and dry, after cooling, extrude through an extruder, cut the extruded strands and cool them with pure water, and obtain components after drying b.
[0040] (2) Composite filament antibac...
Embodiment 2
[0042] The preparation steps of the 80 / 20 side-by-side silver-plated hollow microsphere composite filament antibacterial fiber are as follows:
[0043] (1) Component B is made of the following raw materials in parts by weight: silver-plated hollow microspheres 17, dispersant 18, PP high polymer chip powder 65.
[0044] Wherein the dispersant is made of the following raw materials in parts by weight: polyvinyl alcohol 16.2, glycerin 1.26, polyvinylpyrrolidone 0.54.
[0045] Preparation method of component B: adopt the preparation method of Example 1 to prepare component B from the above raw materials.
[0046] (2) Composite filament antibacterial fiber: use PP high polymer chips as component A, prepare component A and component B through a composite melt spinning machine equipped with composite spinning components to prepare silver-coated hollow microbead composite filament Silk antibacterial fiber, the composite type of this embodiment is 80 / 20 (A / B) parallel type.
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