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Method for preparing six-core MgB2 superconducting wire by magnesium diffusion method

A technology of superconducting wire and diffusion method is applied in the field of preparation of 6-core MgB2 superconducting wire, which can solve the problems of incapable of industrialized production, complicated process and high equipment requirements, and achieves enhanced mechanical properties, increased area, and increased densification degree. Effect

Inactive Publication Date: 2014-07-30
BAOSHENG SCI & TECH INNOVATION
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Although people in the multi-core MgB 2 Great achievements have been made in the preparation of wire strips, but they are still in the experimental stage in the laboratory, and the equipment requirements are high and the process is complicated, so they cannot be used for industrial production and meet the needs of practical applications.

Method used

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  • Method for preparing six-core MgB2 superconducting wire by magnesium diffusion method

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029]Step 1: Install a fixed-core magnesium rod 5 with a diameter of 4mm and a purity greater than 99.8% between the pressure rollers 4 on the left and right sides of the coiler 3, and install the upper end of the fixed-core magnesium rod 5 on the discharge of the special long-necked hopper 6 Below the mouth, the lower end of the special long-necked hopper is located 10cm below the welding machine, and the niobium strip 1 with a width of 35mm and a thickness of 1.5mm is sent to the coiler 3 to be rolled into a niobium tube 2, and the lower end of the niobium tube 2 is shaped by a mold Fix the fixed-core magnesium rod at the center of the niobium tube 2, and then fill the hopper 6 with amorphous boron powder with a purity of not less than (greater than or equal to) 99% and nano-SiC powder with a purity of not less than (greater than or equal to) 99.8% Composed of mixed powder, the mixed powder flows into the niobium tube 2, wherein the mixed powder composed of amorphous boron p...

Embodiment 2

[0035] Step 1: Install a fixed-core magnesium rod 5 with a diameter of 5mm and a purity greater than 99.8% between the pressure rollers 4 on the left and right sides of the coiler 3, and install the upper end of the fixed-core magnesium rod 5 on the discharge of the special long-necked hopper 6 Below the mouth, the lower end of the special long-necked hopper is located 15cm below the welding machine, and the niobium strip 1 with a width of 40mm and a thickness of 2mm is sent to the tube coiler 3 to be rolled into a niobium tube 2, and the lower end of the niobium tube 2 is rolled by a shaping abrasive The fixed core magnesium rod is fixed in the center of the niobium tube 2, and then the mixed powder composed of amorphous boron powder with a purity of not less than 99% and nano-SiC powder with a purity of not less than 99.8% is loaded into the hopper 6, and the mixed powder flows into the niobium tube 2 Among them, the mixed powder composed of amorphous boron powder and nano-Si...

Embodiment 3

[0041] Step 1: Install a fixed-core magnesium rod 5 with a diameter of 4.5mm and a purity greater than 99.8% between the pressure rollers 4 on the left and right sides of the coiler 3, and install the upper end of the fixed-core magnesium rod 5 on the outlet of the special long-necked hopper 6 Below the feed port, the lower end of the special long-necked hopper is located 12cm below the welding machine, and the niobium strip 1 with a width of 38mm and a thickness of 1.8mm is sent to the coiler 3 to be rolled into a niobium tube 2, and the lower end of the niobium tube 2 is shaped by grinding Fix the fixed core magnesium rod in the center of the niobium tube 2, and then fill the hopper 6 with a mixed powder composed of amorphous boron powder with a purity of not less than 99% and nano-SiC powder with a purity of not less than 99.8%, and the mixed powder flows into the niobium In the tube 2, the mixed powder composed of amorphous boron powder and nano-SiC powder is configured acc...

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Abstract

The invention discloses a method for preparing a six-core MgB2 superconducting wire by a magnesium diffusion method. The preparing method comprises the steps that first, a niobium strip coil is manufactured to be a niobium tube, amorphous boron and SiC mixed powder are filled into the niobium tube with a metal magnesium rod being used as a centering rod, and continuous groove rolling is conducted to obtain single-core wires; second, a Cu-Nb composite rod and the single-core wires are placed in an oxygen-free Cu tube to be assembled to obtain a secondary composite body, and the six-core wire is manufactured by route processing through the technology with drawing and rolling combined; third, the two ends of the six-core wire are sealed to be protected and then are coiled, and then the six-core wire is placed on a stainless steel plate, phase heat processing is conducted in an annealing furnace, and the six-core MgB2 superconducting wire through magnesium diffusion is obtained. The core wire of the wire prepared by the method is higher in compactness, meanwhile, uneven tubulating caused by human factors is avoided, the tubulating process is suitable for full-automatic mechanical operation, mass production is facilitated while the evenness of tubulated powder is guaranteed, and therefore the production efficiency of the wire is greatly improved.

Description

Technical field [0001] The present invention belongs to the field of superconducting material processing engineering technology, which involves a 6 -core MGB 2 Preparation method of superconducting wire material. Background technique [0002] MGB 2 Due to the high critical temperature (TC = 39K), large coherent length, and no weak connection of the crystal world due to its critical temperature (TC = 39K), the preparation of its line belt materials has always been the focus of research in various research groups at home and abroad, and the choice of packaging materials is the choice of packaging materials.For the problem that prepare high -performance wire bands is a problem that must be solved, the package materials must be able to withstand certain strength and bending, and have superior thermal stability and low cost. At the same time, it is necessary to avoid chemical reactions with the original powder., To ensure that high critical current density is obtained. [0003] Curren...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): H01B13/00H01B12/10
CPCY02E40/60
Inventor 白质明李成山黄崇祺房权生庞玉春邹红飞徐云海
Owner BAOSHENG SCI & TECH INNOVATION
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