A kind of modification method of guar polysaccharide gum
A guar polysaccharide and modification technology, which is applied in the field of modification of guar polysaccharide gum, can solve the problems of turbidity of polysaccharide gum aqueous solution, well plugging by fracturing fluid, affecting application, etc., and achieves reduction of water-insoluble matter content and good compatibility. , the effect of less water consumption
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Embodiment 1
[0022] Embodiment 1 protease treatment guar polysaccharide gum
[0023] according to figure 1 The process flow diagram of the modification method of guar polysaccharide gum shown, the guar polysaccharide gum is modified.
[0024] 1. Add the guar polysaccharide film with a water insoluble content of 24.8% to the protease aqueous solution for hydration treatment for 30 minutes, the solid-liquid ratio is 1:1.1, and the protease dosage is 30U / g.
[0025] 2. After hydration, extrude the fully swollen film into a snowflake shape on a three-roll machine, and transfer the extruded guar polysaccharide gum into a homogeneous reactor for 6 hours at a temperature of 50°C.
[0026] 3. After the reaction is finished, carry out inactivation treatment in a sterilizing pot, the inactivation temperature is 121° C., and the time is 20 minutes.
[0027] 4. After the inactivation is completed, dry the protease-treated guar polysaccharide gum in an oven at 60° C. for 3 hours.
[0028] 5. The wat...
Embodiment 2
[0029] Embodiment 2 protease treatment guar polysaccharide gum
[0030] The difference between this embodiment and embodiment 1 is only: the dosage of protease is 50U / g;
[0031] After protease treatment, the water-insoluble content of the guar polysaccharide gum was detected, and the result was 17.7%.
Embodiment 3
[0032] Embodiment 3 protease treatment guar polysaccharide gum
[0033] The difference between this embodiment and embodiment 1 is only: the amount of protease is 100U / g;
[0034] After protease treatment, the water-insoluble content of guar polysaccharide gum was detected, and the result was 16.8%.
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