The present application relates to the
chemical industry field, disclose a kind of
reaction system and reaction method,
reaction system includes the reaction kettle, rectifying column, cooler, liquid separator tank and product tank connected in sequence, reaction kettle includes closed kettle body, kettle body has
reaction zone, the blocking plate is arranged in the kettle body of upper portion of this
reaction zone, the gas hole for
gas passing is opened in the blocking plate, product tank is installed with local liquid level display meter, the reaction kettle in the
reaction system provided by the present application is closed kettle body, it is favorable to improve the security of reaction, and kettle body is equipped with blocking plate, when reaction
raw material sublimes, it is condensed into
snowflake when ascending to kettle upper portion region, the
raw material condensed after sublimation can be blocked by blocking plate, avoid its plugging kettle top pipeline, simultaneously
gas phase can be exported in time by rectifying column, cooler, liquid separator tank and stored in product tank, by real-time acquisition the amount of
liquid phase product in product tank, conversion rate can be calculated and obtained.