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42results about How to "Low water insoluble content" patented technology

Temporary plugging diversion agent for refracturing of oil-water well and preparation method thereof

The invention relates to a temporary plugging diversion agent for refracturing of an oil-water well and a preparation method thereof. The temporary plugging diversion agent comprises the following raw materials: adhesive bonding agent 35-65%, plasticizer 15-25%, thickening agent 10-20%, and dispersant 10-20% calculated by the total weight of the temporary plugging diversion agent. The invention also provides the preparation method of the temporary plugging diversion agent, which comprises the following steps: preparing partial thickening agent into a thickening agent water solution; dissolving the adhesive bonding agent into the thickening agent water solution; holding constant temperature in a 25-35 DEG C water bath for 2-5 hours, and after the adhesive bonding agent is swollen completely, increasing the temperature to 45-55 DEG, and continuing holding constant temperature for 0.5-2 hours; after the adhesive bonding agent is completely dissolved, adding dispersant and stirring to be homogenous, and adding the plasticizer and the rest thickening agent while stirring to obtain viscous paste; and cutting the viscous paste to granules of side length 3-6 mm, and drying to obtain the temporary plugging diversion agent. The temporary plugging diversion agent provided by the invention has the advantages of good oil solubility and water solubility, low residue content, good elasticity, and on the like.
Owner:PETROCHINA CO LTD

Method for continuously producing water-soluble monoammonium phosphate by using wet-process phosphoric acid

The invention discloses a method for continuously producing water-soluble monoammonium phosphate by using wet-process phosphoric acid. The method comprises the following steps: adding phosphoric ore pulp to wet-process dilute phosphoric acid; after natural sedimentation, carrying out neutralization reaction between clear desulfurated dilute phosphoric acid at the top and ammonia gas, wherein the neutralization degree of slurry is 0.95-1.05; carrying out natural sedimentation of the neutralized slurry in a settlement trough; filtering ammonium phosphate supernatant in a filter; concentrating and drying the obtained supernatant, so as to prepare the water-soluble monoammonium phosphate, wherein a filter cake and filter residue which are obtained after filtering can be used for preparing an agricultural compound fertilizer. According to the method, the problem of a traditional method that corresponding impurity removal depth can be reached by means of improving the neutralization degree of the slurry and carrying out neutralization reaction many times is avoided, neutralization reaction is carried out only once, and operation is facilitated. Meanwhile, the production efficiency is also improved, the obtained water-soluble monoammonium phosphate is good in quality, and the content of insoluble matter is low. In addition, the method is short in technological process and relatively simple in production control and can be put into continuous production easily.
Owner:云南云天化国际化工有限公司

Temporary plugging diversion agent for refracturing of oil-water well and preparation method thereof

The invention relates to a temporary plugging diversion agent for refracturing of an oil-water well and a preparation method thereof. The temporary plugging diversion agent comprises the following raw materials: adhesive bonding agent 35-65%, plasticizer 15-25%, thickening agent 10-20%, and dispersant 10-20% calculated by the total weight of the temporary plugging diversion agent. The invention also provides the preparation method of the temporary plugging diversion agent, which comprises the following steps: preparing partial thickening agent into a thickening agent water solution; dissolving the adhesive bonding agent into the thickening agent water solution; holding constant temperature in a 25-35 DEG C water bath for 2-5 hours, and after the adhesive bonding agent is swollen completely, increasing the temperature to 45-55 DEG, and continuing holding constant temperature for 0.5-2 hours; after the adhesive bonding agent is completely dissolved, adding dispersant and stirring to be homogenous, and adding the plasticizer and the rest thickening agent while stirring to obtain viscous paste; and cutting the viscous paste to granules of side length 3-6 mm, and drying to obtain the temporary plugging diversion agent. The temporary plugging diversion agent provided by the invention has the advantages of good oil solubility and water solubility, low residue content, good elasticity, and on the like.
Owner:PETROCHINA CO LTD

Water-soluble compound microbial fertilizer and preparation method thereof

The invention belongs to the technical field of microbial fertilizers, and particularly relates to a water-soluble compound microbial fertilizer and a preparation method thereof. The water-soluble compound microbial fertilizer provided by the invention comprises yeast fermentation waste liquid dry powder, inorganic water-soluble fertilizer and functional bacteria powder in a mass ratio of (68-85):(15-30): (0.3-3.5). According to the water-soluble compound microbial fertilizer provided by the invention, the water-soluble yeast fermentation waste liquid dry powder is used as an organic carrier,so that the defect that the traditional compound microbial fertilizer is not water-soluble is overcome, the application mode of the compound microbial organic fertilizer is expanded, meanwhile, the damage of the traditional organic fertilizer to crops is avoided, and by compounding the water-soluble yeast fermentation waste liquid dry powder with the functional bacterium powder and the inorganicwater-soluble fertilizer according to a certain proportion, the soil fertility can be effectively improved. Experimental results of the embodiment show that the content of the water-insoluble substances in the water-soluble compound microbial fertilizer provided by the invention is 0.08%-0.25%, and the requirement that the content of the water-insoluble substances in a general water-soluble fertilizer standard is less than or equal to 5% is met.
Owner:FUJIAN SANJU BIOLOGICAL SCI & TECH

Production process for organic water-soluble fertilizer

The invention discloses a production process for an organic water-soluble fertilizer. The production process comprises the following steps: S1, adding agricultural organic wastes into a crushing machine for crushing operation, and carrying out filtering and collecting a sieved substance for subsequent usage; S2, adding organic fertilizer raw materials into water, carrying out heating under stirring, and adding organic active substances into a mixed solution for complete biological activation; S3, carrying out filtering so as to remove suspended matters from the mixed solution, and adding KOH into the solution so as to adjust the acidity and alkalinity of an organic liquid; S4, adding medium elements and trace elements into the organic matter mixed solution with high activity in proportion,and carrying out a reaction; and S5, placing a reacted solution in an ultrasonic environment for action, then carrying out coating through a coating machine, fully heating the mixed solution, and carrying out complete drying so as to obtain the organic water-soluble fertilizer. The production process provided by the invention is convenient to operate; and the organic water-soluble fertilizer produced by using the production process provided by the invention is greatly improved in economic values due to low content of water-insoluble substances contained in raw materials.
Owner:甘肃天元化工有限公司

The method for preparing carboxymethyl hydroxypropyl guar gum powder by one-step method of guar gum sheet

The invention relates to a method for preparing carboxymethyl hydroxypropyl guar gum powder by a guar gum sheet one-step method. The method comprises the following steps of adding guar gum sheets into an organic solvent-water mixed solution, heating the solution to a temperature of 30-80 DEG C, adding a sodium hydroxide solution into the heated mixed solution, carrying out an alkalization reaction process for 2-60min, then adding an etherifying agent into the reaction product, carrying out a reaction process at a temperature of 30-80 DEG C for 30-180min, then carrying out cooling and filtration, washing the filter residue, carrying out crushing, and carrying out drying to obtain a finished product. The method utilizes cheap guar gum sheets as raw materials, realizes carboxymethyl and hydroxyalkyl etherification modification by the one-step method, and greatly shortens reaction time than a multi-step method. Through synchronization of carboxymethylation and hydroxyalkylation, processes are simple and convenient, reaction time is short, and the product has low water-insoluble substance content, good crosslinking performances, good fracture initiation and sand-carrying functions and good application prospects in the field of oil field pressing crack liquids. The method has a wide application prospect in the field of oil field auxiliary agents.
Owner:山东广浦生物科技有限公司

Special solid water-soluble fertilizer for coptis chinensis and preparation method thereof

The invention discloses a special solid water-soluble fertilizer for coptis chinensis and a preparation method thereof. The special solid water-soluble fertilizer for coptis chinensis comprises the following raw materials by weight percentage: 50-65% of water-soluble ammonium polyphosphate, 10-15% of potassium nitrate, 10-15% of ammonium dihydrogen phosphate, 10-15% of dipotassium hydrogen phosphate and 3-10% of urea; the total nutrient content of the fertilizer reaches 76% or more, and the aggregated phosphorus accounts for 65% or more of the total phosphorus. The long-term sustained releaseof water-soluble ammonium polyphosphate is combined with the quick-acting effect of ordinary water-soluble fertilizers such as potassium dihydrogen phosphate, potassium nitrate, ammonium dihydrogen phosphate and urea to provide sufficient nutrients for each growth stage of coptis chinensis; the absorption and utilization rate of fertilizer nutrients is high, the loss of fertilizer nutrients is less, environmental pollution caused by conventional water-soluble fertilizers is lowered, the manual work is saved, the yield is increased, fertilization costs are reduced, and the planting efficiency is improved.
Owner:SHIFANG CHANGFENG CHEM CO LTD

Method for producing polyaluminium chloride

ActiveCN102070170BReduce manufacturing costIn line with the environmental protection concept of energy saving and emission reductionAluminium chloridesWater/sewage treatment by flocculation/precipitationIngotPolyaluminium chloride
The invention relates to a method for producing polyaluminium chloride, which comprises the following steps: adding aluminum-containing waste residue into solution of hydrochloric acid and reacting at 90 to 120 DEG C and under a normal pressure for 3 to 5 hours; filtering, collecting mother solution, filling the mother solution into an acid-resistance and vapor-heated reactor with a stirring device, starting stirring, supplying a proper amount of water, starting to add calcium aluminate powder, and after the addition is finished, regulating the density of feed liquid to more than or equal to 1.20g / ml with water; and adding a synergist, heating and keeping the temperature between 90 and 120 DEG C, reacting at normal temperature for 3 to 5 hours, and obtaining finished liquid polyaluminium chloride. Compared with the prior art, the method, which uses aluminum-containing waste residue obtained after the neutralization of waste liquid from surface pickling of aluminum ingots and bands as raw material, reduces the manufacturing cost of polyaluminium chloride, recycles aluminum-containing waste residue and is in accordance with the environmental-protection concept of energy conservationand emission reduction.
Owner:蓝保(厦门)水处理科技有限公司
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