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High-impermeability epoxy powder paint and preparation method thereof

An epoxy powder and permeability technology, used in powder coatings, epoxy resin coatings, anti-corrosion coatings, etc., can solve problems such as weak permeability resistance, and achieve strong adhesion, good permeability resistance, and good scratch resistance. Effect

Active Publication Date: 2014-09-03
洛阳双瑞防腐工程技术有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0011] In order to solve the problem of weak penetration resistance of epoxy powder coatings, the invention provides a high penetration resistance epoxy powder coating for pipeline anticorrosion and its preparation method, the high penetration resistance epoxy powder coating prepared by the preparation method , with high penetration resistance, strong adhesion, scratch resistance, excellent anti-corrosion performance, long anti-corrosion life, etc.

Method used

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  • High-impermeability epoxy powder paint and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0047] A kind of high impermeability epoxy powder coating proportion by weight is: 50 parts of GESR904H, 9 parts of HB310, 0.1 part of 2-methylimidazole, 6 parts of titanium dioxide, 24 parts of precipitated barium sulfate, 400 mesh sieved wet 8 parts of French sericite powder, 1 part of nano-silica, 1 part of polybutylacrylate adsorbed by silica, 0.7 part of polylauryl methacrylate, 0.1 part of 2-hydroxy-1,2-diphenylethanone Parts, fumed silica 0.1 part.

[0048] When preparing:

[0049] The speed of the pre-mixer was controlled at 1300 r / min, and the pre-mixing time was controlled at 5 min.

[0050] The temperature of zone I of the twin-screw extruder is set at 110°C, the temperature of zone II is set at 97°C, the temperature of zone III is set at 70°C, and the extruder is preheated for 1 hour after the temperature reaches the set temperature.

[0051] For other unmentioned preparation methods, please refer to the technical scheme.

Embodiment 2

[0053] A kind of high impermeability epoxy powder coating proportion by weight is: 58 parts of GESR904H, 10.5 parts of HB310, 0.3 part of 2-methylimidazole, 4.5 parts of titanium dioxide, 17 parts of precipitated barium sulfate, 800 mesh sieved wet 6 parts of French sericite powder, 1.5 parts of nano-titanium dioxide, 0.8 parts of polybutyl acrylate adsorbed by silica, 0.9 parts of polylauryl methacrylate, 0.3 parts of 2-hydroxy-1,2-diphenylethanone, 0.2 parts of fumed silica.

[0054] When preparing:

[0055] The speed of the pre-mixer was controlled at 1400 r / min, and the pre-mixing time was controlled at 4 minutes.

[0056] The temperature in zone I of the twin-screw extruder is set at 115°C, the temperature in zone II is set at 94°C, and the temperature in zone III is set at 65°C. After the temperature reaches the set temperature, the extruder is preheated for 1 hour.

[0057] For other unmentioned preparation methods, please refer to the technical scheme.

Embodiment 3

[0059] A kind of high impermeability epoxy powder coating proportioning by weight is: 65 parts of GESR904H, 12 parts of HB310, 0.5 part of 2-methylimidazole, 3 parts of titanium dioxide, 10 parts of precipitated barium sulfate, 800 mesh sieved wet 4 parts of French sericite powder, 3 parts of nano-montmorillonite, 0.7 parts of polybutyl acrylate adsorbed by silica, 1 part of polylauryl methacrylate, 0.5 parts of 2-hydroxy-1,2-diphenylethanone parts, fumed silica 0.3 parts.

[0060] When preparing:

[0061] The speed of the pre-mixer is controlled at 1500 r / min, and the time of pre-mixing is controlled at 3 min.

[0062] The temperature in zone I of the twin-screw extruder is set to 120°C, the temperature in zone II is set to 90°C, and the temperature in zone III is set to 60°C. After the temperature reaches the set temperature, the extruder is preheated for 0.5h.

[0063] For other unmentioned preparation methods, please refer to the technical scheme.

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Abstract

High-impermeability epoxy powder paint comprises, in parts by weight, 50-65 parts of high-purity bisphenol A type solid epoxy resin, 9-12 parts of hydroxyl resin, 0.1-0.5 part of 2-methylimidazole, 3-6 parts of titanium dioxide, 10-24 parts of precipitated barium sulphate, 4-8 parts of wet-process sericite powder, 1-3 parts of a nanometer filling material, 0.7-1 part of poly(butyl acrylate), 0.7-1 part of poly(cauryl methacrylate), 0.1-0.5 part of 2-hydroxy-2-phenylacetophenone and 0.1-0.3 part of fumed silica. The high-impermeability epoxy powder paint is prepared by performing premixing, fusion extrusion, tabletting and milling. The high-impermeability epoxy powder paint is good in impermeability, strong in adhesive force, good in scratch resistance, excellent in corrosion resistance, long in corrosion-resistant life and applicable to corrosion prevention of metal pipes subjected to liquid-medium corrosion or in gas-medium high-corrosivity environment.

Description

[0001] technical field [0002] The invention belongs to the technical field of powder coatings, and in particular relates to a high-penetration-resistant epoxy powder coating and a preparation method thereof. Background technique [0003] Powder coating is a recognized high production efficiency, excellent coating performance, eco-friendly, economical coating product, and its VOC emission is almost zero. With the improvement of social requirements for environmental protection, powder coatings have developed rapidly, and their proportion in the field of industrial anticorrosion is increasing. Epoxy powder coatings are a kind of powder coatings. Due to their strong adhesion and excellent physical properties , good electrical insulation, and high corrosion resistance are widely used in the field of pipeline corrosion protection. [0004] At present, the epoxy powder coatings on the market are mainly used in the anti-corrosion of buried pipelines. The environment is harsh, a...

Claims

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Application Information

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IPC IPC(8): C09D163/02C09D7/12C09D5/03C09D5/08B29C69/00B29C47/92B29C43/00B29C48/92
CPCB29C47/92B29C47/6087B29C2947/92657B29C48/40B29C48/625B29C48/92B29C2948/92561B29C2948/9259B29C2948/92657B29C2948/92704
Inventor 张延奎黄伯和郭佳效苏松峰
Owner 洛阳双瑞防腐工程技术有限公司