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Copper antioxidant and preparation method thereof

An antioxidant and hydrogen peroxide technology, applied in the field of copper antioxidants and antioxidants, can solve the problems of short anti-oxidation time and high cost of copper powder antioxidants, and achieve the effects of good protection, low odor and excellent stability

Inactive Publication Date: 2014-09-17
BOLINDA SCI TECH SHENZHEN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the cost of preparing copper powder antioxidants in the prior art is high, and the antioxidation time of the prepared copper powder antioxidants is short

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0017] A copper antioxidant provided by the present invention contains the following components per liter of copper antioxidant: 50 g of hydroxyethylidene diphosphonic acid, 100 g of ethanol, 80 g of hydrogen peroxide, 40 g of benzotriazole, and 10 g of isothiocyanate , 15g of lauryl sulfate, 10g of sodium molybdate, and 12g of sodium tripolyphosphate.

[0018] The preparation method is as follows:

[0019] 1) each component is weighed by the above-mentioned mass number;

[0020] 2) Put the components weighed in step 1) into the reactor, add water to 1 L, and then stir at room temperature for 10 minutes to obtain the copper antioxidant.

Embodiment 2

[0022] A copper antioxidant provided by the present invention contains the following components per liter of copper antioxidant: 50 g of hydroxyethylidene diphosphonic acid, 100 g of ethanol, 50 g of hydrogen peroxide, 20 g of benzotriazole, and 20 g of isothiocyanate , dodecyl sulfate 8g, sodium molybdate 20g, sodium tripolyphosphate 8g.

[0023] The preparation method is as follows:

[0024] 1) each component is weighed by the above-mentioned mass number;

[0025] 2) Put the components weighed in step 1) into the reactor, add water to 1L, and then stir at room temperature for 12 minutes to obtain the copper antioxidant.

Embodiment 3

[0027] A copper antioxidant provided by the present invention contains the following components per liter of copper antioxidant: 70g of hydroxyethylidene diphosphonic acid, 70g of ethanol, 100g of hydrogen peroxide, 30g of benzotriazole, and 15g of isothiocyanate , lauryl sulfate 10g, sodium molybdate 15g, sodium tripolyphosphate 10g.

[0028] The preparation method is as follows:

[0029] 1) each component is weighed by the above-mentioned mass number;

[0030] 2) Put the components weighed in step 1) into the reactor, add water to 1L, and then stir at room temperature for 15 minutes to obtain the copper antioxidant.

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PUM

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Abstract

The invention discloses a copper antioxidant and a preparation method thereof and belongs to the technical field of metal anti-oxidation. According to the copper antioxidant and the preparation method thereof, the copper antioxidant is good in protective property and does not corrode for a long time and does not fade. The copper antioxidant is characterized in that the copper antioxidant per liter contains the following ingredients by weight: 50-100g of hydroxy ethylidene diphosphonic acid, 50-100g of ethanol, 80-150g of hydrogen peroxide, 20-40g of a corrosion inhibitor, 10-20g of isothiocyanate, 8-15g of alkyl sulfate, 10-20g of sodium molybdate, 8-12g of sodium tripolyphosphate and the balance of water. The preparation method of the copper antioxidant comprises the steps: (1) weighing all the ingredients; (2) putting the ingredients weighed in the step (1) in a reaction vessel, adding water until the volume is 1L, and then, stirring for 20-60 minutes at the temperature of 40-50 DEG C, thereby obtaining the copper antioxidant.

Description

technical field [0001] The invention relates to an antioxidant, in particular to a copper antioxidant and belongs to the technical field of metal oxidation resistance. Background technique [0002] Copper metal has good luster, and its electrical conductivity is almost equal to that of silver, but the price is only one-twentieth of silver. Therefore, in terms of cost performance, copper powder is an ideal conductive filler. These characteristics of copper powder make it widely used in conductive adhesives, conductive plastics, conductive coatings and other fields. However, the fine copper powder has a large specific surface area, active chemical properties, and is prone to oxidation in the air, resulting in darkening of the material and poor decoration, and the oxide is an insulator, which makes it difficult for conductive materials to be used for a long time. Maintain good electrical conductivity. Therefore, how to prevent copper powder from being oxidized during the prep...

Claims

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Application Information

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IPC IPC(8): C23F11/14
Inventor 宋云
Owner BOLINDA SCI TECH SHENZHEN
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