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Solid sodium lactate low-temperature granulation method

A low-temperature granulation and sodium lactate technology, which is applied in the separation/purification of carboxylic acid compounds, organic chemistry, etc., can solve the problems of only 17% thermal efficiency utilization rate of dry hot air and difficult process, and achieve good color and equipment productivity Improve efficiency and overcome the effect of easy adhesion

Active Publication Date: 2014-11-05
武汉三江航天固德生物科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The thermal efficiency utilization rate of dry hot air in the drying process is only 17%;
[0005] 2. During the hot air drying process, since the moisture in the material needs to be vaporized and separated before the material can be solidified, the process is difficult, and the production capacity of the unit equipment is not higher than 1.0 kg / m3 equipment space

Method used

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  • Solid sodium lactate low-temperature granulation method

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Effect test

Embodiment 1

[0021] A low-temperature granulation method of solid sodium lactate, comprising the following steps:

[0022] 1) The sodium lactate solution is evaporated under reduced pressure using a wiped film evaporator. Before evaporation, the content of sodium lactate is 40wt%. Controlled at 0.04MPa, the concentration process can be completed within 5 minutes;

[0023] 2) Press the concentrated solution into the rotary centrifugal spray granulator through compressed air. At this time, the temperature of the concentrated solution is 91°C, so that the concentrated solution is sprayed downward from the high-speed rotating disk on the upper part of the granulator. , the speed of the centrifugal disc is 10,000 rpm; at the same time, the cold air of 5°C is introduced from the top of the granulator synchronously to control the ventilation volume, and the temperature is not higher than 45°C when the cold air is drawn out from the lower side of the granulator; the liquid droplets Cool and solid...

Embodiment 2

[0025] A low-temperature granulation method of solid sodium lactate, comprising the following steps:

[0026] 1) Evaporate the sodium lactate solution under reduced pressure using a wiped film evaporator. The content of sodium lactate before evaporation is 46wt%. When evaporating, the jacket heating steam of the wiped film evaporator is 0.25MPa. When evaporating, the temperature inside the wiped film evaporator is controlled at 92°C, and the pressure is controlled at a negative pressure of 0.045MPa. The concentration process can be completed within 5 minutes Finish;

[0027] 2) Introduce the concentrated solution into the centrifugal spray granulator. At this time, the temperature of the concentrated solution is 91°C, so that the concentrated solution is sprayed downward from the rotating centrifugal disc of the granulator. Cool air at 10°C is introduced from the top of the granulator, and the ventilation volume is controlled. When the cold air is drawn out from the lower sid...

Embodiment 3

[0029] A low-temperature granulation method of solid sodium lactate, comprising the following steps:

[0030] 1) Evaporate the sodium lactate solution under reduced pressure using a wiped film evaporator. Before evaporation, the content of sodium lactate is 47wt%. , the pressure is controlled at a negative pressure of 0.05MPa;

[0031] 2) Introduce the concentrated solution into the centrifugal spray granulator. At this time, the temperature of the concentrated solution is 91°C, so that the concentrated solution is sprayed downward from the rotating centrifugal disc of the granulator. Cool air at 14°C is introduced above the granulator to control the ventilation rate. When the cold air is drawn out from the lower side of the granulator, the temperature is not higher than 45°C; after heat exchange between the cold air and the concentrated solution, solid crystalline powder of sodium lactate is formed and falls into the chassis. , Complete the granulation of solid sodium lactat...

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Abstract

The invention provides a solid sodium lactate low-temperature granulation method. The method comprises the following steps: (1) a sodium lactate solution is subjected to reduced-pressure evaporation by using a thin-film evaporator, wherein sodium lactate content in the solution is increased to 90-92wt% within 5min; and the obtained solution is discharged. During the reduced-pressure evaporation process, the pressure of the jacket heating steam of the thin-film evaporator is controlled at 0.2-0.4MPa, the temperature in the thin-film evaporator is controlled at above 90 DEG C, and the pressure in the thin-film evaporator is controlled at 0.04-0.05MPa; (2) the concentrated solution is pressed into a rotating centrifugation spray granulation machine through compressed air, and the temperature of the concentrated solution is maintained at above 90 DEG C, such that the concentrated solution is spayed as a mist from a high-speed rotation disk on the upper part of the granulation machine; at a same time, cold air with a temperature of 4-15 DEG C is synchronously delivered from above the granulation machine, and the temperature of cold air delivered out from the lower side part of the granulation machine is no higher than 45 DEG C; liquid mist is subjected to heat-exchange with the cold air, and is cooled and solidified, such that sodium lactate solid crystallized powder is obtained. According to the invention, low-temperature granulation is adopted, such that production efficiency is high, and heat energy utilization rate is greatly improved. The method is suitable for popularization and production.

Description

technical field [0001] The invention relates to the field of lactic acid products, in particular to a low-temperature granulation method of solid sodium lactate. Background technique [0002] Sodium lactate is a natural food additive widely used in many countries in Asia, Europe and the United States. It is considered as a "safe and non-toxic substance" by the US Food and Drug Administration. It can be used as an emulsifier, humectant, flavor improver, quality improver, antioxidant synergist and pH regulator, and is widely used in the meat and poultry food processing industry. It can enhance the flavor, inhibit the growth of pathogenic bacteria in food, and prolong the shelf life of products. [0003] When traditional sodium lactate is granulated, the method adopted is to use 60% sodium lactate solution and send it into a spray fluidized bed drying granulator to spray and dry it. The existing defects are: [0004] 1. The semi-finished liquid sodium lactate solution has a r...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C51/43C07C51/42C07C59/08
CPCC07C51/42C07C51/43C07C59/08
Inventor 赵文胜谢剑宏张金彬梁庭德徐仁义
Owner 武汉三江航天固德生物科技有限公司
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