Radiation curable and thermosettable resin composition, and dry film solder resist
A thermosetting resin and resin composition technology, applied in the field of DFSR, light-curing and thermosetting resin composition and solder mask dry film, can solve the problem that solder resist does not show, can not meet PCT tolerance, TCT heat resistance HAST resistance, high glass transition temperature and other issues, to achieve the effect of superior PCT resistance, improved heat resistance reliability, high glass transition temperature
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Embodiment 1
[0168] By combining the cyanate group of the bisphenol cyanate compound BA-230 available from Lonza Co., Ltd. with acrylic acid and 1,2,3,6-tetrahydrophthalic acid (4-cyclohexene -1,2-dicarboxylic acid) was reacted at a molar ratio of 1:1 to obtain an iminocarbonate compound as an acid-modified oligomer.
[0169] 10% by weight of the above iminocarbonate compounds, 25% by weight of ZAR-2000 (Nippon Kayaku Co., Ltd.) were mixed as other acid-modified oligomers, and 5% by weight of DPHA (SK Cytec Co., Ltd.) .) As a photopolymerizable monomer, 2% by weight of TPO as a photoinitiator, 15% by weight of YDCN-500-80P (Nippon Kayaku Co., Ltd.) as a thermosetting adhesive, 0.4% by weight of 2-PI As a thermosetting binder catalyst, 23% by weight of filler BaSO4, 0.3% by weight of pigment phthalocyanine blue, 0.3% by weight of additive BYK-110 and 19% by weight of solvent DMF, a resin composition was prepared.
[0170] A dry film consisting of a carrier film, a photosensitive film (thickness...
Embodiment 2 and 3
[0173] The dry film and the printed circuit board were prepared according to the same steps as in Example 1, except that 5 wt% (Example 2) or 15 wt% (Example 3) of iminocarbonate compounds were used, and according to The amount of amino carbonate compounds increases or decreases the amount of solution.
Embodiment 4 to 6
[0175] The dry film and the printed circuit board were prepared according to the same steps as in Example 1, except that 5% by weight of T-1420 (Nippon Kayaku Co., Ltd.; Example 4), DPCA-60 (Nippon Kayaku Co., Ltd.; Example 5) or R-684 (Nippon Kayaku Co., Ltd.; Example 6) was used as a photopolymerization monomer instead of 5 wt% of DPHA (SK Cytec Co., Ltd.).
[0176] The specific compositions of the resin compositions of Examples 1 to 6 are summarized in Table 1 below.
[0177] [Table 1]
[0178]
[0179]
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