Application of miRNA-30a in preparation of diagnostic reagents as marker molecules
A technology of 1.mirna-30a and 5.mirna-30a, which is applied in the field of biomedicine and can solve the problems of variable factors, poor stability and specificity, etc.
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Embodiment 1
[0040] Example 1 Chip screening of target miRNA specifically expressed in human kidney
[0041] 1. Construction of CI-AKI rat model
[0042] The present invention establishes a CI-AKI rat model by injecting a hypotonic contrast agent through the tail vein on the basis of water deprivation for 3 days and diuretic "pretreatment". This is a new type of CI-AKI rat model established by the inventors, and the specific protocol can be found in relevant literature (Sun SQ, et al. Int Journal of Cardiol 172(2014) e48-50).
[0043] 2. Differential expression profile analysis of miRNA microarray
[0044] 1) miRNA chip preparation
[0045] On the basis of successful modeling using the above method, plasma and kidneys of CI-AKI rats were collected 8 hours after modeling for sample loading on the chip. Using Agilent miRNAs 10.0version chip technology, plasma and kidney total RNA were used for loading, and phosphorylated Cyanine3-pCp was used for labeling, followed by chip hybridization, ...
Embodiment 2
[0053] Example 2 Verification of the specific expression of the target miRNA kidney
[0054] The total RNA of rat tissues was extracted by the classic Trizol method, and real-time PCR was used to detect the expression levels of target miRNAs in rat tissues. At the same time, the expression levels of human tissues were compared by searching published literature on the expression profile of miRNAs in human tissues. figure 2 It is the result of the expression profile of miRNA-30a in each tissue of rat (A) and human (B). The expression of miRNA-30a in the kidney of rat and human is 2 times or more than that of other organs, so it is considered that the miRNA kidney specificity is high.
Embodiment 3
[0055] Example 3 Extraction of plasma microRNA
[0056] The present invention adopts the two-step centrifugation method to blood plasma, has removed blood cell and cell debris in blood, and RNA extraction adopts mirVana PARIS Kit (Applied Biosystem, P / N AM1556), and this is a kind of RNA that is applicable to blood plasma or serum. Reagent test kit. At present, there is no recognized internal reference for RNA quantification in plasma. In the present invention, an exogenous internal reference cel-miR-39 (miRNA expressed by nematodes, which is not expressed in the human body) is added to the RNA extraction process to correct RT-PCR detection results of target miRNAs.
[0057] Plasma sample pretreatment method: collect whole blood in EDTA anticoagulant tubes (working concentration: 1.8mg / ml), first centrifuge at 4°C, 820g for 10min to remove blood cells, and then centrifuge the supernatant at 4°C, 16000g for 10min to remove cells Finally, pipette the supernatant into a 1.5ml R...
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