Application of continuously prepared rubber masterbatch to sidewall rubber of car tire
A technology for rubber masterbatch and car tires, applied in special tires, vehicle parts, tire parts, etc., can solve the problems of low heat generation, reduced mixing steps, and difficulty in dispersion, and achieve low heat generation and reduced mixing. Steps to solve the effect that is not easy to disperse
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Embodiment 1
[0058] Add 12 parts of white carbon black, 1 part of silane coupling agent, 8 parts of naphthenic oil and 2 parts of anti-aging agent 264 into 60 parts of n-hexane solution of cis-butadiene gum, after mixing, pour it into the coagulator continuously for coagulation, and then Solvent removal and drying afforded masterbatch 1-1. Add 45 parts of carbon black N660 to 40 parts of natural rubber in n-hexane solution, mix, inject continuously into the coagulator for coagulation, and then remove solvent and dry to obtain masterbatch 1-2.
[0059] Add masterbatch 1-1 and masterbatch 1-2 to the internal mixer according to the ratio of total rubber 100phr, mix evenly, add 3 parts of zinc oxide, 1.5 parts of stearic acid, 3 parts of anti-aging agent 4020, 2 parts of protective wax , 2 parts of octyl phenolic tackifying resin, after mixing, the next piece, parked for 8 hours, then added to the internal mixer and mixed evenly, after adding 0.75 parts of accelerator NS, 1.8 parts of sulfur, ...
Embodiment 2
[0061] 12 parts of white carbon black, 1 part of silane coupling agent, 8 parts of naphthenic oil, 2 parts of antioxidant 264, 3 parts of zinc oxide, 1.5 parts of stearic acid, 3 parts of antioxidant 4020, 2 parts of protective wax, octyl Add 2 parts of phenolic tackifying resin to 60 parts of n-hexane solution of butadiene rubber, mix, pour into the coagulator continuously for coagulation, and then remove solvent and dry to obtain masterbatch 2-1. Add 45 parts of carbon black N660 to 40 parts of natural rubber in n-hexane solution, mix, inject continuously into the coagulator for coagulation, and then remove solvent and dry to obtain masterbatch 2-2.
[0062] Add masterbatch 2-1 and masterbatch 2-2 to the internal mixer according to the ratio of total rubber 100phr, mix evenly, add 0.75 parts of accelerator NS, 1.8 parts of sulfur, and mix, after mixing, pass the roller and lower the sheet After the mixed rubber was parked for 8 hours, it was vulcanized to positive vulcanizat...
Embodiment 3
[0066] 50 parts of white carbon black, 4 parts of silane coupling agent, 8 parts of naphthenic oil, 2 parts of antioxidant 264, 3 parts of zinc oxide, 1.5 parts of stearic acid, 3 parts of antioxidant 4020, 2 parts of protective wax, octyl 2 parts of phenolic tackifying resin were added to 60 parts of butadiene rubber and 40 parts of natural rubber in n-hexane solution, after mixing, they were continuously poured into the coagulator for coagulation, and then the solvent was removed and dried to obtain masterbatch 3.
[0067] Add masterbatch 3 to the internal mixer evenly, add 0.75 parts of accelerator NS, 1.8 parts of sulfur, and then mix. After mixing, roll off the sheet. After the mixed rubber is parked for 8 hours, use a flat vulcanizer at 165 ° C. After down vulcanization to positive vulcanization, the vulcanizate 3 is prepared continuously. Tire 195 / 60R14 was prepared using continuous sidewall compound 3.
[0068] Table 4 Test performance of sidewall vulcanizate prepared...
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